Lee Wei-Fang, Takahashi Hidekazu, Iwasaki Naohiko, Peng Pei-Wen
School of Dental Technology, Taipei Medical University, Taipei, 11031, Taiwan.
School of Oral Health Engineering, Faculty of Dentistry, Tokyo Medical and Dental University, Tokyo, 113-8549, Japan.
Clin Oral Investig. 2023 Jan;27(1):165-171. doi: 10.1007/s00784-022-04704-6. Epub 2022 Sep 20.
There is insufficient information about the effects of the thickness of externally characterized stains or glazes on CIELAB color parameters and the translucency parameter (TP) of 5 mol% yttria partially stabilized zirconia (5Y-PSZ). The present study evaluated the effect of a thickness reduction of the externally characterized or glazed layer on its CIE2000 color parameters and TP of 5Y-PSZ.
Twenty-eight specimens were sectioned from 5Y-PSZ blanks. Three brands of powdered stains (namely VI, SH, and IV) and a glaze (GL) were used to extrinsically stain the specimen surfaces (n = 7 per group). After measuring the final thickness and color, specimens of each group were carefully ground and finally polished. The reduced thickness was carefully controlled in decrements of 0.02 mm on the characterized stains or glazed layers at each reduction cycle until the surface of the un-stained zirconia was exposed. The CIELAB color parameters of specimens were measured using a spectrophotometer. Subsequently, differences in lightness (∆L'), chroma (∆C'), and hue (∆H'), and TP values and color differences (ΔE) were calculated using the CIEDE2000 formula to determine differences between the specimen and the un-stained zirconia at each reduction cycle. A paired-samples t-test, two-way mixed-design analysis of variance, and Pearson correlation coefficient were used to analyze the data (α = 0.05).
There were no significant differences in lightness, chroma, hue, or TP values before or after glazing or after each reduction cycle of the glazed layer. Mean ΔE values ranged between 20.94 and 33.55 after applying the externally characterized stains. With a decreased thickness of the characterized stain layer, there were observed that significant decreases in ∆L', ∆H', ∆C', and ΔE, and significant increases in TP.
Increasing the thickness of externally characterized stains decreased the lightness and caused the alternation of chroma and hue, whereas these phenomena were not observed in the glazed group. There was a slight change of CIE2000 color parameters and TP when the thickness of the characterized layer exceeded 0.06 mm.
The application and thickness of externally characterized stains can sensitively affect CIE2000 color parameters and translucency of 5Y-PSZ.
关于外部特征色料或釉料的厚度对5摩尔%氧化钇部分稳定氧化锆(5Y-PSZ)的CIELAB颜色参数和半透明度参数(TP)的影响,目前信息不足。本研究评估了外部特征层或釉面层厚度减小对其CIE2000颜色参数和5Y-PSZ的TP的影响。
从5Y-PSZ坯体上切割出28个试样。使用三个品牌的粉末色料(即VI、SH和IV)和一种釉料(GL)对试样表面进行外部着色(每组n = 7)。在测量最终厚度和颜色后,对每组试样进行仔细研磨并最终抛光。在每个减少周期,对特征色料或釉面层以0.02毫米的递减量仔细控制厚度减小,直至未着色氧化锆表面暴露。使用分光光度计测量试样的CIELAB颜色参数。随后,使用CIEDE2000公式计算明度(∆L')、彩度(∆C')和色调(∆H')的差异以及TP值和颜色差异(ΔE),以确定每个减少周期试样与未着色氧化锆之间的差异。采用配对样本t检验、双向混合设计方差分析和Pearson相关系数分析数据(α = 0.05)。
在施釉前后或釉面层每个减少周期后,明度、彩度、色调或TP值均无显著差异。施加外部特征色料后,平均ΔE值在20.94至33.55之间。随着特征色料层厚度的减小,观察到∆L'、∆H'、∆C'和ΔE显著降低,而TP显著增加。
增加外部特征色料的厚度会降低明度并导致彩度和色调的变化,而在釉料组中未观察到这些现象。当特征层厚度超过0.06毫米时,CIE2000颜色参数和TP有轻微变化。
外部特征色料的应用和厚度会敏感地影响5Y-PSZ的CIE2000颜色参数和半透明度。