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抗菌纳米填充复合材料的无创适应性评估。

Noninvasive Adaptation Appraisal of Antimicrobial Nano-Filled Composite.

机构信息

Department of Restorative Dentistry, Faculty of Dentistry, King Abdulaziz University, Jeddah, Saudi Arabia; Department of Oral Biology, Faculty of Dentistry, Cairo University, Cairo, Egypt.

Department of Restorative Dentistry, Faculty of Dentistry, King Abdulaziz University, Jeddah, Saudi Arabia.

出版信息

Int Dent J. 2023 Aug;73(4):533-541. doi: 10.1016/j.identj.2022.11.004. Epub 2022 Dec 21.

Abstract

OBJECTIVE

The aim of this research was to assess the effect of incorporating zein-coated magnesium oxide (zMgO) nanofillers to resin-based composite on the internal adaptation of the restorations using cross-polarisation optical coherence tomography (CP-OCT).

METHODS

Thirty noncarious human molar teeth were used. Class V cavities (3 × 5 mm) were prepared on the buccal and lingual surfaces of each tooth. Clearfil SE Bond 2 was applied to all the cavities and then the teeth were divided into 3 groups (n = 10) as follows: group 1-restored with N-Flow composite; group 2 and group 3-restored with N-Flow composite mixed with different zMgO nanoparticle concentrations (0.3% and 0.5% by weight, respectively) and then light cured using an LED curing device. Specimens were examined for interfacial adaptation examination under CP-OCT. Characterisation of the dental composite incorporating zMgO was done by Fourier-transform infrared spectroscopy (FTIR), x-ray diffraction (XRD), and field emission scanning electron microscopy (FESEM). Results were analysed with Kruskall-Wallis test followed by Mann-Whitney U test, at a significance level of P < .05.

RESULTS

XRD spectra exhibited the sharp peaks of zMgO in the composite enhanced with zMgO nanoparticles. FESEM analysis showed a uniform distribution of the zMgO nanoparticles in the composite and FTIR illustrated no change in the spectra. The gap percentage along the cavity floor was significantly lower in groups 2 and 3 in comparison to group 1 (P < .05). Also there was a significant difference in gap percentages between groups 2 and 3 (P < .05), with group 3 showing the lowest gap percentage.

CONCLUSIONS

The incorporation of 0.3% and 0.5% zMgO nanoparticles in flowable composite assists in improving the internal adaptation of the composite to the tooth surface.

摘要

目的

本研究旨在评估在基于树脂的复合材料中加入玉米醇溶蛋白涂层氧化镁(zMgO)纳米填料对使用交叉偏振光相干断层扫描(CP-OCT)评估修复体内部适应性的影响。

方法

本研究使用 30 颗非龋恒磨牙。在每颗牙齿的颊面和舌面制备 3×5mm 的 V 类洞。所有窝洞均涂布 Clearfil SE Bond 2,然后将牙齿分为 3 组(n=10):组 1 用 N-Flow 复合树脂修复;组 2 和组 3 用 N-Flow 复合树脂分别与不同浓度的 zMgO 纳米颗粒(重量比分别为 0.3%和 0.5%)混合,然后使用 LED 固化装置光固化。用 CP-OCT 对试件进行界面适应性检查。用傅里叶变换红外光谱(FTIR)、X 射线衍射(XRD)和场发射扫描电子显微镜(FESEM)对掺入 zMgO 的牙科复合材料进行了表征。采用 Kruskal-Wallis 检验和 Mann-Whitney U 检验对结果进行分析,检验水准为 P <.05。

结果

XRD 谱图显示复合材料中增强 zMgO 纳米颗粒的 zMgO 具有尖锐的峰。FESEM 分析显示 zMgO 纳米颗粒在复合材料中分布均匀,FTIR 图谱无变化。与组 1 相比,组 2 和组 3 沿窝洞底部的间隙百分比显著降低(P <.05)。组 2 和组 3 之间的间隙百分比也有显著差异(P <.05),其中组 3 的间隙百分比最低。

结论

在流动性复合树脂中加入 0.3%和 0.5%的 zMgO 纳米颗粒有助于提高复合树脂与牙面的内部适应性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7c88/10350601/8e31e3f50c08/gr1.jpg

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