Jeong Hyunjo, Shin Hyojeong, Zhang Shuzeng, Li Xiongbing
Department of Mechanical Engineering, Wonkwang University, Iksan 54538, Republic of Korea.
Graduate School of Flexible and Printable Electronics, Jeonbuk National University, Jeonju 54896, Republic of Korea.
Materials (Basel). 2023 Jun 18;16(12):4453. doi: 10.3390/ma16124453.
Harmonic generation measurement is recognized as a promising tool for inspecting material state or micro-damage and is an ongoing research topic. Second harmonic generation is most frequently employed and provides the quadratic nonlinearity parameter (β) that is calculated by the measurement of fundamental and second harmonic amplitudes. The cubic nonlinearity parameter (β2), which dominates the third harmonic amplitude and is obtained by third harmonic generation, is often used as a more sensitive parameter in many applications. This paper presents a detailed procedure for determining the correct β2 of ductile polycrystalline metal samples such as aluminum alloys when there exists source nonlinearity. The procedure includes receiver calibration, diffraction, and attenuation correction and, more importantly, source nonlinearity correction for third harmonic amplitudes. The effect of these corrections on the measurement of β2 is presented for aluminum specimens of various thicknesses at various input power levels. By correcting the source nonlinearity of the third harmonic and further verifying the approximate relationship between the cubic nonlinearity parameter and the square of the quadratic nonlinearity parameter (β∗β), β2≈β∗β, the cubic nonlinearity parameters could be accurately determined even with thinner samples and lower input voltages.
谐波产生测量被认为是一种用于检测材料状态或微观损伤的有前途的工具,并且是一个正在进行研究的课题。二次谐波产生是最常使用的,它提供了通过测量基波和二次谐波振幅来计算的二次非线性参数(β)。三次谐波产生所主导的三次谐波振幅的三次非线性参数(β2),在许多应用中通常被用作更敏感的参数。本文提出了一种详细的程序,用于在存在源非线性的情况下确定韧性多晶金属样品(如铝合金)的正确β2。该程序包括接收器校准、衍射和衰减校正,更重要的是对三次谐波振幅进行源非线性校正。针对不同厚度的铝试样在不同输入功率水平下,展示了这些校正对β2测量的影响。通过校正三次谐波的源非线性,并进一步验证三次非线性参数与二次非线性参数平方之间的近似关系(β∗β),即β2≈β∗β,即使使用更薄的样品和更低的输入电压,也能够准确确定三次非线性参数。