Czujko Tomasz, Gajda Daniel, Rindfleisch Matt, Babij Michał, Zaleski Andrzej
Institute of Materials Science and Engineering, Military University of Technology, Kaliskiego 2, 00-908 Warsaw, Poland.
Institute of Low Temperature and Structure Research, Polish Academy of Sciences (PAS), Okolna 2, 50-422 Wrocław, Poland.
Materials (Basel). 2023 Sep 11;16(18):6157. doi: 10.3390/ma16186157.
The use of a low annealing temperature during the production of coils made from superconducting materials is very important because it reduces the production costs. In this study, the morphology, transport critical-current density (), irreversible magnetic field (), and critical temperature () of straight wires and small 2% C-doped MgB coils were investigated. The coils were made using the wind-and-react (W&R) method and annealed at various temperatures from 610 °C to 650 °C for 2-12 h. Critical-current measurements were made for both the coils and straight wires at the temperatures of 4.2 K, 20 K, 25 K, and 30 K. During our research study, we determined the process window that provides the best critical parameters of the coils (annealing at a temperature of 650 °C for 6 h). Moreover, we observed that small coils made with unreacted MgB wire and then annealed had morphology and critical parameters similar to those of straight 2% C-doped MgB wires. Moreover, small-diameter bending of 20 mm and 10 mm did not lead to transverse cracks, which can cause a large reduction in in the coils. This indicates that the processes of optimization of thermal treatment parameters can be carried out on straight MgB wires for MgB superconducting coils.
在由超导材料制成的线圈生产过程中使用低退火温度非常重要,因为这会降低生产成本。在本研究中,对直导线以及含2% C掺杂的MgB小线圈的形态、输运临界电流密度()、不可逆磁场()和临界温度()进行了研究。这些线圈采用绕线 - 反应(W&R)方法制作,并在610℃至650℃的不同温度下退火2至12小时。在4.2K、20K、25K和30K的温度下对线圈和直导线进行了临界电流测量。在我们的研究过程中,我们确定了能提供线圈最佳临界参数的工艺窗口(在650℃下退火6小时)。此外,我们观察到,由未反应的MgB线制成然后退火的小线圈,其形态和临界参数与含2% C掺杂的直MgB线相似。而且,20mm和10mm的小直径弯曲并未导致横向裂纹,而横向裂纹会使线圈中的大幅降低。这表明,可以在用于MgB超导线圈的直MgB线上进行热处理参数的优化过程。