Zeng Zhizhong, Shang Jian, Lin Dan
School of Materials Science and Engineering, Liaoning University of Technology, Jinzhou, China.
Heliyon. 2024 Feb 2;10(3):e25452. doi: 10.1016/j.heliyon.2024.e25452. eCollection 2024 Feb 15.
The surface of AISI 52100 steel was pre-treated by laser remelting with different powers, and the vanadizing layer were prepared on remelted steel by pack cementation. The microstructure and properties of vanadizing layer were investigated by XRD, microhardness tester, metallographic microscope, scanning electron microscope, energy dispersive spectrometer, friction and wear tester. The critical load L was determined by observing the micro-scratch morphology of scratches through micro-scratch experiments, and its wear performance was studied. The results show that the hardness of remelting zone increase with the increase of laser power. When the laser power is 500 W, the microhardness is 424.6 HV. The vanadizing layer formed on the remelting surfaces is uniform and dense. The layers are mainly composed of VC phase and α-Fe/α'-Fe phase, the VC phase has the preferred orientation of (200) and (111) planes. There is a good metallurgical bonding between the vanadizing layer and the steel, and the thickness is 2.7 μm-12.15 μm, the microhardness is 2050.7 HV-2350.9 HV. When the laser remelting power is 300 W, the vanadizing layer is better in thickness, microhardness and average friction coefficient, the bonding force Lc between the vanadizing layer and the substrate is about 41.59 N, and the main failure mode is the spalling of the vanadizing layer. It can be concluded that laser remelting pre-treatment can greatly improve the hardness and wear resistance.
采用不同功率的激光重熔对AISI 52100钢表面进行预处理,并通过包埋渗金属法在重熔后的钢表面制备渗钒层。利用X射线衍射仪、显微硬度计、金相显微镜、扫描电子显微镜、能谱仪、摩擦磨损试验机对渗钒层的组织和性能进行了研究。通过微划痕试验观察划痕的微观划痕形貌确定临界载荷L,并研究其磨损性能。结果表明,重熔区硬度随激光功率的增加而增大。当激光功率为500W时,显微硬度为424.6HV。在重熔表面形成的渗钒层均匀致密。渗钒层主要由VC相和α-Fe/α'-Fe相组成,VC相具有(200)和(111)晶面的择优取向。渗钒层与基体之间存在良好的冶金结合,厚度为2.7μm-12.15μm,显微硬度为2050.7HV-2350.9HV。当激光重熔功率为300W时,渗钒层在厚度、显微硬度和平均摩擦系数方面表现较好,渗钒层与基体之间的结合力Lc约为41.59N,主要失效模式为渗钒层剥落。可以得出结论,激光重熔预处理可以大大提高硬度和耐磨性。