Department of Chemical and Materials Engineering, New Mexico State University, Las Cruces, NM 88003.
Department of Chemical and Materials Engineering, New Mexico State University, Las Cruces, NM 88003; Department of Family and Consumer Sciences, New Mexico State University, Las Cruces, NM 88003; Center of Excellence in Sustainable Food and Agricultural Systems, New Mexico State University, Las Cruces, NM 88003.
J Dairy Sci. 2024 Aug;107(8):5473-5480. doi: 10.3168/jds.2024-24657. Epub 2024 Apr 11.
The meltdown test is an efficient tool widely and commonly used to characterize structural changes in frozen desserts resulting from different ingredients and processing conditions. The meltdown is commonly determined by a gravimetric test, and it is used to obtain the onset (M), rate (M), and maximum (M) meltdown. However, these parameters are calculated ambiguously due to inconsistencies in the methodology. This work aims to model the meltdown curves (weight vs. time) of different commercial frozen dessert samples (36 commercial samples). Samples of commercial frozen desserts (40-60 g) was placed on a 304 stainless wire cloth (1.50 mm opening size and 52% open area) suspended ∼15 cm above an analytical balance, and the dripped portion of the melted sample was continuously recorded throughout the duration of the test. The meltdown test was conducted at room temperature. Each meltdown test generated between 3,000 to 4,000 data points and was modeled using 4 equations: the logistic model, the Gompertz model, the Richard model, and the Hill model. All the meltdown curves were sigmoidal in shape, regardless of the type of frozen dessert. The experimental meltdown curves were adequately represented by the logistic model, judging by several criteria (R = 0.999, R = 0.999, Akaike information criterion = 6,582, and F-value = 1.88 × 10). Thus, the logistic model was shown to be an effective tool for predicting the meltdown curves of frozen desserts, and it can be used to unambiguously define M, M, and M. Moreover, a dimensionless response (meltdown behavior, M) that combines M, M, and M was developed and used for mapping the meltdown of different commercial frozen desserts.
融霜测试是一种有效的工具,广泛用于描述不同成分和加工条件下冷冻甜点的结构变化。融霜通常通过重量测试来确定,用于获得起始(M)、速率(M)和最大(M)融霜。然而,由于方法学上的不一致,这些参数的计算存在歧义。本工作旨在对不同商业冷冻甜点样品(36 个商业样品)的融霜曲线(重量与时间)进行建模。将商业冷冻甜点样品(40-60 g)置于 304 不锈钢丝布(开口尺寸为 1.50 毫米,开口面积为 52%)上,悬停在分析天平上方约 15 厘米处,融化样品的滴落部分在测试过程中连续记录。融霜测试在室温下进行。每个融霜测试产生 3000 到 4000 个数据点,并使用 4 个方程进行建模:逻辑模型、戈珀兹模型、理查德模型和希尔模型。无论冷冻甜点的类型如何,所有融霜曲线均呈 S 形。根据几个标准(R = 0.999、R = 0.999、Akaike 信息准则 = 6.582 和 F 值 = 1.88×10),逻辑模型可以很好地表示实验融霜曲线。因此,逻辑模型被证明是预测冷冻甜点融霜曲线的有效工具,可用于明确定义 M、M 和 M。此外,还开发了一个无量纲响应(融霜行为,M),该响应结合了 M、M 和 M,用于绘制不同商业冷冻甜点的融霜情况。