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从火龙果(Hylocereus polyrhizus)果皮中提取的果胶及其在可食用膜中的应用。

Pectin extracted from red dragon fruit (Hylocereus polyrhizus) peel and its usage in edible film.

机构信息

School of Food Science and Technology, Jiangnan University, Wuxi 214122, China.

Food Technology Department, Faculty of Engineering, Bina Nusantara University, Jakarta 11480, Indonesia.

出版信息

Int J Biol Macromol. 2024 Sep;276(Pt 1):133804. doi: 10.1016/j.ijbiomac.2024.133804. Epub 2024 Jul 10.

Abstract

Pectin was extracted from red dragon fruit (Hylocereus polyrhizus) peel using two different extraction methods: subcritical water extraction (SCWE) and conventional acid extraction (AE), from two different types of peels, fresh peel puree and dried peel powder. SCWE method on fresh peel puree showed an ∼18.88 % increase in pectin yield compared to AE. Extracted pectin is classified as low methoxyl pectin (DE: 8.51-50.64 %), with an average molecular weight ranging from 115.23 kDa to 577.84 kDa and a Gal-A content of 44.09 % - 53.90 %. The potential of pectin from fresh peel puree to be applied as a biodegradable film was further explored. Different pectin concentrations (3-5 % w/v) were used to prepare the films. Regarding the film performance, PF-S5, which was produced from SCWE with 5 % of pectin concentration, exhibits better thermal stability (T 250 °C, residue of 28.69 %) and higher moisture barrier (WVP 5.59 × 10 g.cm.s.Pa). In comparison, PF-A showed lower water solubility (45.14-69.15 %), higher water contact angle (33.01° - 44.35°), and better mechanical properties (TS: 2.12-4.11 MPa, EB: 48.72-61.39 %). Higher molecular weight accompanied by higher DE and Gal-A content contributes to better pectin film properties.

摘要

从火龙果(Hylocereus polyrhizus)果皮中使用两种不同的提取方法:亚临界水提取(SCWE)和传统酸提取(AE),从两种不同类型的果皮中提取果胶,即新鲜果皮泥和干燥果皮粉。与 AE 相比,SCWE 法在新鲜果皮泥中的果胶得率提高了约 18.88%。提取的果胶被分类为低甲氧基果胶(DE:8.51-50.64%),平均分子量范围从 115.23 kDa 到 577.84 kDa,Gal-A 含量为 44.09%-53.90%。进一步探索了来自新鲜果皮泥的果胶作为可生物降解膜的应用潜力。使用不同的果胶浓度(3-5%w/v)制备薄膜。关于薄膜性能,PF-S5 是由 SCWE 制备的,其中果胶浓度为 5%,表现出更好的热稳定性(T 250°C,残留物为 28.69%)和更高的水分阻隔性(WVP 5.59×10 g.cm.s.Pa)。相比之下,PF-A 具有较低的水溶性(45.14-69.15%)、较高的水接触角(33.01°-44.35°)和更好的机械性能(TS:2.12-4.11 MPa,EB:48.72-61.39%)。较高的分子量伴随着较高的 DE 和 Gal-A 含量有助于改善果胶膜的性能。

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