Department of Studies in Physics, Manasagangotri, University of Mysore, Mysuru 570006, India.
Department of Chemistry, J.S.S College of Arts, Commerce and Science, Mysuru 570006, India.
Radiat Prot Dosimetry. 2024 Jul 17;200(11-12):1216-1219. doi: 10.1093/rpd/ncae080.
Latent fingerprint developed at the site of crime is considered as crucial physical evidence in forensic investigation. The mixed metal oxides (MXOY, M = Ba, Zn, Al, Ce) nanophosphor was synthesised by irradiating the precursor solution with 60Co gamma radiation followed by solution combustion method. The structural, morphological, optical characteristics and fingerprint imaging were studied using X-ray diffraction (XRD), scanning electron microscopy, UV-visible spectroscopy and powder dusting method, respectively. The XRD results revealed that the average crystallite size is found to be 30 nm with the estimated bandgap of 3.18 eV. The broadband UV exited luminescence of the phosphors was observed at λMax = 330 nm. The PL spectrum shows three emission bands at 432, 444 and 460 nm that corresponds to blue regions, suggesting that the synthesised nanophosphor is a potential luminous material for latent fingerprinting and luminescent devices.
在犯罪现场形成的潜在指纹被认为是法医学调查中的关键物理证据。通过用 60Co 伽马射线辐照前驱体溶液,然后采用溶液燃烧法合成混合金属氧化物(MXOY,M=Ba、Zn、Al、Ce)纳米荧光粉。分别采用 X 射线衍射(XRD)、扫描电子显微镜、紫外-可见分光光度计和粉末散布法研究了结构、形态、光学特性和指纹成像。XRD 结果表明,平均晶粒尺寸为 30nm,估算的能带隙为 3.18eV。在 λMax=330nm 处观察到了磷光体的宽带紫外激发发光。PL 光谱在 432、444 和 460nm 处显示三个发射带,对应于蓝色区域,表明合成的纳米荧光粉是潜在指纹和发光器件的潜在发光材料。