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大气压等离子体清洗的不锈钢电极的表面分析

Surface Analysis of Stainless Steel Electrodes Cleaned by Atmospheric Pressure Plasma.

作者信息

Zhang Jia, Dang Mengjia, Luo Cheng, Ba Yongshan, Li Qingkai

机构信息

School of Aerospace Science and Technology, Xidian University, Xi'an 710126, China.

出版信息

Materials (Basel). 2024 Jul 22;17(14):3621. doi: 10.3390/ma17143621.

Abstract

The Z-pinch device is a critical component in inertial confinement fusion, where stainless steel electrodes must withstand high current densities of up to MA/cm. Gases and difficult-to-remove impurities adhering to the electrode surfaces can ionize, significantly impacting the device's electrical conductivity efficiency. In this paper, the surface of stainless steel electrodes was subjected to cleaning using a large-area plasma jet under atmospheric pressure. The wettability, chemical composition, and chemical state of the electrode surface were characterized using a water contact angle measuring instrument and X-ray photoelectron spectroscopy (XPS). The cleaning effect under different discharge parameters was systematically analyzed. The results revealed a significant reduction in the content of carbon pollutants on the surface of stainless steel electrodes, decreasing from 62.95% to a minimum of 37.68% after plasma cleaning. Moreover, the water contact angle decreased from 70.76° to a minimum of 29.31°, and the content of water molecules adsorbed on the surface decreased from 17.31% to a minimum of 5.9%. Based on the evolution process of micro-element content and chemical state on the surface of stainless steel electrode, the cleaning process of adhering substances on the surface by atmospheric pressure plasma was analyzed by the layered cleaning model for surface pollutants on stainless steel.

摘要

Z箍缩装置是惯性约束聚变中的关键部件,其中不锈钢电极必须承受高达MA/cm的高电流密度。附着在电极表面的气体和难去除杂质会发生电离,显著影响装置的导电效率。本文采用大气压下的大面积等离子体射流对不锈钢电极表面进行清洗。使用水接触角测量仪和X射线光电子能谱(XPS)对电极表面的润湿性、化学成分和化学状态进行了表征。系统分析了不同放电参数下的清洗效果。结果表明,不锈钢电极表面的碳污染物含量显著降低,等离子体清洗后从62.95%降至最低37.68%。此外,水接触角从70.76°降至最低29.31°,表面吸附的水分子含量从17.31%降至最低5.9%。基于不锈钢电极表面微量元素含量和化学状态的演变过程,采用不锈钢表面污染物分层清洗模型分析了大气压等离子体对表面附着物质的清洗过程。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/75a9/11278598/e86146d2549f/materials-17-03621-g001.jpg

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