Alegre Jesús Manuel, Díaz Andrés, García Ruben, Peral Luis Borja, Lorenzo-Bañuelos Miriam, Cuesta Isidoro Iván
Escuela Politécnica Superior, University of Burgos, Av de Cantabria s/n, 09006 Burgos, Spain.
HIP Innovation Center, Hiperbaric S.L., C. Condado de Treviño, 6, 09001 Burgos, Spain.
Materials (Basel). 2024 Aug 2;17(15):3825. doi: 10.3390/ma17153825.
Binder jetting 3D printing is an additive manufacturing technique based on the creation of a part through the selective bonding of powder with an adhesive, followed by a sintering process at high temperature to densify the material and produce parts with acceptable properties. Due to the high initial porosity in the material after sintering, which is typically around 5%, post-sintering treatments are often required to increase the material density and enhance the mechanical and fatigue properties of the final component. This paper focuses on the study of the benefits of hot isostatic pressing (HIP) after sintering on the mechanical and fatigue properties of a binder jetting Ti-6Al-4V alloy. Two different HIP processes were considered in this study: one at 920 °C/100 MPa for 4 h, and a second at a higher pressure but lower temperature (HIP-HPLT) at 850 °C/200 MPa for 2 h. The effects of the HIP on the densification, microstructure, mechanical behavior, and fatigue properties were investigated. The results show that the HIP-HPLT process produced a significant increase in the mechanical and fatigue properties of the material compared with the as-sintered parts and even with the conventional HIP process. However, the fatigue and fracture micromechanisms suggest that the oxygen content, which resulted from the decomposition of the binder during the sintering process, played a critical role in the final mechanical properties. Oxygen could reduce the ductility and fatigue life, which deviated from the behavior observed in other additive manufacturing techniques, such as powder bed fusion (PBF).
粘结剂喷射3D打印是一种增材制造技术,其原理是通过用粘合剂选择性地粘结粉末来制造零件,随后进行高温烧结过程以使材料致密化,并生产出具有可接受性能的零件。由于烧结后材料中的初始孔隙率较高,通常约为5%,因此通常需要进行烧结后处理以提高材料密度,并增强最终部件的机械性能和疲劳性能。本文重点研究烧结后热等静压(HIP)对粘结剂喷射Ti-6Al-4V合金的机械性能和疲劳性能的益处。本研究考虑了两种不同的HIP工艺:一种是在920℃/100MPa下保温4小时,另一种是在较高压力但较低温度(HIP-HPLT)下在850℃/200MPa下保温2小时。研究了HIP对致密化、微观结构、力学行为和疲劳性能的影响。结果表明,与烧结态零件相比,甚至与传统HIP工艺相比,HIP-HPLT工艺使材料的机械性能和疲劳性能有了显著提高。然而,疲劳和断裂微观机制表明,烧结过程中粘合剂分解产生的氧含量对最终机械性能起着关键作用。氧会降低延展性和疲劳寿命,这与粉末床熔融(PBF)等其他增材制造技术中观察到的行为不同。