Zhang Zhan, Zhang Xiaojun, Lin Bing, Zhong Yaqian, Zhang Wenxiu, Zhong Shangrong, Chen Xiaxia
College of Food and Pharmacy, Zhejiang Ocean University, Zhoushan, 316022, China.
Zhejiang Marine Fisheries Research Institute, Zhoushan, 316021, China.
Food Chem X. 2024 Nov 15;24:102012. doi: 10.1016/j.fochx.2024.102012. eCollection 2024 Dec 30.
This study aims to prepare and characterize cinnamaldehyde-loaded zein/sodium alginate nanoparticles (ZCNPs) and incorporate them into polyvinyl alcohol/chitosan (PVA/CS) bioactive films (PSCN) to investigate their compatibility, physicochemical properties, and their application as a preservation material for pomfret fish. The results indicate that the anionic sodium alginate coating improved the particle size, zeta potential, and PDI of zein nanoparticles. The ZCNPs were uniformly dispersed within the films, enhancing the mechanical properties and water vapor barrier performance. The X-ray diffraction (XRD) and Fourier transform infrared (FTIR) analyses confirmed the amorphous structure of the films and the formation of hydrogen bonds. In the PVA/CS film, with the increase of ZCNPs, the thermal decomposition temperature of the film increased from 298 °C to 308 °C, while the film thickness and water contact angle were not significantly affected, remaining around 0.31 cm and 23°, respectively. Additionally, after the incorporation of ZCNPs, the DPPH radical scavenging rate of the film increased from 14.58 % to 95.38 %, significantly delaying the quality deterioration of pomfret during storage.
本研究旨在制备并表征负载肉桂醛的玉米醇溶蛋白/海藻酸钠纳米颗粒(ZCNPs),并将其掺入聚乙烯醇/壳聚糖(PVA/CS)生物活性膜(PSCN)中,以研究它们的相容性、理化性质及其作为鲳鱼保鲜材料的应用。结果表明,阴离子海藻酸钠涂层改善了玉米醇溶蛋白纳米颗粒的粒径、zeta电位和PDI。ZCNPs均匀分散在薄膜中,增强了薄膜的机械性能和水蒸气阻隔性能。X射线衍射(XRD)和傅里叶变换红外(FTIR)分析证实了薄膜的无定形结构和氢键的形成。在PVA/CS薄膜中,随着ZCNPs含量的增加,薄膜的热分解温度从298℃升高到308℃,而,而薄膜厚度和水接触角未受到显著影响,分别保持在0.31cm左右和23°左右。此外,掺入ZCNPs后,薄膜的DPPH自由基清除率从14.58%提高到95.38%,显著延缓了鲳鱼在储存期间的品质劣化。