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利用绿色预处理技术从胡萝卜渣中提取微晶纤维素并进行表征。

Extraction and characterization of microcrystalline cellulose from carrot pomace using green pretreatment technologies.

作者信息

Meral Hilal, Demirdöven Aslıhan

机构信息

Tokat Gaziosmanpasa University, Faculty of Engineering and Architecture, Food Engineering Dept., 60150 Tokat, Turkey.

出版信息

Food Chem. 2025 Mar 15;468:142429. doi: 10.1016/j.foodchem.2024.142429. Epub 2024 Dec 12.

Abstract

In this study, microcrystalline cellulose (MCC) from carrot pomace, which is a byproduct of the carrot process, was produced. The Response Surface Methodology optimized the effectiveness of autoclaving & ultrasonic pretreatments (AUP) in MCC extraction with a D-optimal design. The yield of AUP was 36.62 % at the optimum point; at the conventional acid hydrolysis method, it was 31.40 %. AUP-derived MCC demonstrated superior rheological properties, including water holding capacity (4.58 g H₂O/g MCC) and oil adsorption capacity (2.94 g oil/g MCC), comparable to commercial MCC. Characterization analyses revealed that the AUP-derived MCC had high crystallinity, thermal stability, and a short-fibered morphology, confirmed by FTIR, SEM, TGA, and XRD. Utilizing carrot pomace reduces agricultural waste while providing a valuable dietary fiber source (87.94 % insoluble fiber). This study highlights MCC production from carrot pomace using AUP offers an economically and environmentally viable alternative, with potential applications in food, pharmaceutical, and cosmetic industries.

摘要

在本研究中,制备了来自胡萝卜加工副产品胡萝卜渣的微晶纤维素(MCC)。响应面法通过D-最优设计优化了高压灭菌和超声预处理(AUP)在MCC提取中的效果。在最佳点,AUP的产率为36.62%;在传统酸水解法中,产率为31.40%。AUP衍生的MCC表现出优异的流变学特性,包括持水能力(4.58 g H₂O/g MCC)和吸油能力(2.94 g油/g MCC),与商业MCC相当。表征分析表明,AUP衍生的MCC具有高结晶度、热稳定性和短纤维形态,这通过傅里叶变换红外光谱(FTIR)、扫描电子显微镜(SEM)、热重分析(TGA)和X射线衍射(XRD)得到证实。利用胡萝卜渣减少了农业废弃物,同时提供了一种有价值的膳食纤维来源(87.94%为不溶性纤维)。本研究强调,采用AUP从胡萝卜渣中生产MCC提供了一种经济且环境可行的替代方案,在食品、制药和化妆品行业具有潜在应用。

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