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用于3D打印的超声改性花生蛋白-瓜尔豆胶复合乳液凝胶的制备与表征

Preparation and Characterization of Ultrasonically Modified Peanut Protein-Guar Gum Composite Emulsion Gels for 3D Printing.

作者信息

Yan Hong-Yan, Zhang Shao-Bing

机构信息

College of Food Science and Engineering, Henan University of Technology, Zhengzhou 450001, China.

出版信息

Gels. 2024 Dec 14;10(12):828. doi: 10.3390/gels10120828.

Abstract

This study aimed to prepare ultrasonically modified peanut protein-guar gum composite emulsion gels for 3D printing. The composition of the composite emulsion gels was determined in single-factor and orthogonal experiments. The results revealed that the optimal composite emulsion gels consisted of 6% peanut protein, 50% oil and 0.2% guar gum. After crushing pretreatment for 45 s, the printing deviation of the composite emulsion gels was reduced to 8.58 ± 0.20%. Moreover, after ultrasonic treatment (200 W for 20 min) of peanut proteins, the obtained composite emulsion gels presented the highest yield stress, hardness and G' values, as well as a denser and more homogeneous microstructure. After protein ultrasonic modification (200 W or 600 W for 20 min), the printing accuracy and self-supporting properties of the composite emulsion gels for printing complex shapes significantly improved, which was attributed to their stronger textural and rheological properties; however, ultrasonically modified peanut protein-guar gum composite emulsion gels were not suitable for printing products with smooth surfaces.

摘要

本研究旨在制备用于3D打印的超声改性花生蛋白-瓜尔豆胶复合乳液凝胶。通过单因素实验和正交实验确定了复合乳液凝胶的组成。结果表明,最佳复合乳液凝胶由6%的花生蛋白、50%的油和0.2%的瓜尔豆胶组成。经过45秒的粉碎预处理后,复合乳液凝胶的打印偏差降低至8.58±0.20%。此外,对花生蛋白进行超声处理(200W,20分钟)后,所得复合乳液凝胶呈现出最高的屈服应力、硬度和G'值,以及更致密、更均匀的微观结构。经过蛋白质超声改性(200W或600W,20分钟)后,用于打印复杂形状的复合乳液凝胶的打印精度和自支撑性能显著提高,这归因于其更强的质地和流变性能;然而,超声改性花生蛋白-瓜尔豆胶复合乳液凝胶不适用于打印表面光滑的产品。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1115/11675485/0844307c7078/gels-10-00828-g001.jpg

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