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通过铸造、铣削和3D打印制造的钴铬牙科合金的力学性能和微观结构评估。

Assessment of mechanical properties and microstructure of Co-Cr dental alloys manufactured by casting, milling, and 3D printing.

作者信息

Schettini Ana, Pesun Igor J, França Rodrigo

机构信息

Graduate student, Graduate Prosthodontics, Department of Restorative Dentistry, Gerald Niznick College of Dentistry, University of Manitoba, Winnipeg, Manitoba, Canada.

Associate Professor and Director, Graduate Prosthodontics, Department of Restorative Dentistry, Gerald Niznick College of Dentistry, University of Manitoba, Winnipeg, Manitoba, Canada.

出版信息

J Prosthet Dent. 2025 Mar;133(3):906.e1-906.e7. doi: 10.1016/j.prosdent.2024.12.017. Epub 2024 Dec 30.

Abstract

STATEMENT OF PROBLEM

The mechanical properties and microstructure of cobalt chromium (Co-Cr) alloys should be considered when choosing the best alloy for each clinical situation. More information is needed on the digital manufacturing methods of metals in dentistry, such as computer numerical control (CNC), and direct laser metal sintering (DMLS).

PURPOSE

The aim of this study was to investigate the effect of the 3 different Co-Cr manufacturing processes on the mechanical properties and microstructure of Co-Cr dental alloys.

MATERIAL AND METHODS

Dumbbell-shaped specimens (n=6) were fabricated using casting (CAST), CNC, and DMLS techniques. Tensile, 3-point bend, and microhardness testing were performed, and the microstructure evaluated through scanning electron microscopy, energy dispersive X-ray analysis, and X-ray diffraction analysis. The ANOVA test followed by post hoc Tukey tests were used for statistical analysis (α=.05).

RESULTS

DMLS showed the greatest values for 0.2% yield strength (908.0 ±13.1 MPa), tensile strength (1123.7 ±6.5 MPa), flexural strength (2273.0 ±43.2 MPa), and microhardness (438.2 ±44.9 HV), followed by CAST and CNC. No statistical differences were found for elongation between CNC and DMLS or DMLS and CAST (P>.05). No statistical differences were found in elastic modulus among all groups (P>.05). EDX revealed a slightly different chemical composition among the groups. XRD showed face-centered cubic as the dominant phase and a small amount of hexagonal close-packed structure in all groups. A peak of σ phase was identified in the CAST group.

CONCLUSIONS

The mechanical properties and microstructures of Co-Cr dental alloys were significantly influenced by the fabrication method used. DMLS and CNC milling produced better products that traditional methods, leading to the improved durability and reliability of dental prostheses. These advancements underscore the importance of selecting appropriate fabrication methods to optimize clinical outcomes and patient satisfaction.

摘要

问题陈述

在为每种临床情况选择最佳合金时,应考虑钴铬(Co-Cr)合金的机械性能和微观结构。对于牙科金属的数字化制造方法,如计算机数控(CNC)和直接激光金属烧结(DMLS),需要更多信息。

目的

本研究的目的是调查3种不同的Co-Cr制造工艺对Co-Cr牙科合金机械性能和微观结构的影响。

材料与方法

使用铸造(CAST)、CNC和DMLS技术制作哑铃形试样(n=6)。进行拉伸、三点弯曲和显微硬度测试,并通过扫描电子显微镜、能量色散X射线分析和X射线衍射分析评估微观结构。采用方差分析(ANOVA)检验,随后进行事后Tukey检验进行统计分析(α=0.05)。

结果

DMLS的0.2%屈服强度(908.0±13.1MPa)、抗拉强度(1123.7±6.5MPa)、抗弯强度(2273.0±43.2MPa)和显微硬度(438.2±44.9HV)值最高,其次是CAST和CNC。CNC与DMLS之间或DMLS与CAST之间的伸长率无统计学差异(P>0.05)。所有组的弹性模量无统计学差异(P>0.05)。EDX显示各组的化学成分略有不同。XRD显示面心立方为主要相,所有组中均有少量六方密堆积结构。在CAST组中鉴定出σ相峰。

结论

Co-Cr牙科合金的机械性能和微观结构受所用制造方法的显著影响。DMLS和CNC铣削生产的产品优于传统方法,从而提高了牙科假体的耐久性和可靠性。这些进展强调了选择合适制造方法以优化临床结果和患者满意度的重要性。

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