采用薄层色谱法和串联质谱法检测及鉴定尿液提取物中的吗啡。
Detection and identification of morphine in urine extracts using thin-layer chromatography and tandem mass spectrometry.
作者信息
Tames F, Watson I D, Morden W, Wilson I D
机构信息
Dept. Clinical Biochemistry, University Hospital, Aintree, Liverpool, UK.
出版信息
J Chromatogr B Biomed Sci Appl. 1999 Jun 11;729(1-2):341-6. doi: 10.1016/s0378-4347(99)00120-6.
The application of tandem mass spectrometry to the analysis and identification of morphine following thin-layer chromatography is described. FAB-mass spectrometry and mass spectrometry-mass spectrometry were performed following chromatography on silica gel high-performance thin-layer chromatography plates. The successful application of this simple methodology to a urine extract suggests that this approach has practical utility for confirming the identity of abused drugs detected by thin-layer chromatography.
描述了串联质谱法在薄层色谱法分析和鉴定吗啡中的应用。在硅胶高效薄层色谱板上进行色谱分析后，进行了快原子轰击质谱法和串联质谱法。这种简单方法在尿液提取物中的成功应用表明，该方法对于确证通过薄层色谱法检测到的滥用药物的身份具有实际用途。
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