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Recognition and quantitation of cis-vaccenic and eicosenoic fatty acids in olive oils by 13C nuclear magnetic resonance spectroscopy.

作者信息

Scano P, Casu M, Lai A, Saba G, Dessi M A, Deiana M, Corongiu F P, Bandino G

机构信息

Dipartimento di Scienze Chimiche, Universita di Cagliari, Complesso Universitario di Monserrato, Cagliari, Italy.

出版信息

Lipids. 1999 Jul;34(7):757-9. doi: 10.1007/s11745-999-0422-4.

DOI:10.1007/s11745-999-0422-4
PMID:10478934
Abstract

The presence of 11-cis monoenoic fatty acids was detected in olive oil samples by means of 13C nuclear magnetic resonance spectroscopy, and the positional isomery on the glycerol backbone was derived. The 11-cis vaccenic and eicosenoic fatty acid resonances were recognized and the amounts of the fatty acids quantified. For comparison purposes, a quantitative analysis was also made by gas chromatography.

摘要

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Dibutyrate derivatization of monoacylglycerols for the resolution of regioisomers of oleic, petroselinic, and cis-vaccenic acids.单酰甘油的丁酸酯衍生化用于拆分油酸、岩芹酸和顺式-异油酸的区域异构体。

本文引用的文献

1
PREPARATION OF FATTY ACID METHYL ESTERS AND DIMETHYLACETALS FROM LIPIDS WITH BORON FLUORIDE--METHANOL.用氟化硼 - 甲醇从脂质制备脂肪酸甲酯和二甲基缩醛
J Lipid Res. 1964 Oct;5:600-8.
2
High-resolution nuclear magnetic resonance spectroscopy--applications to fatty acids and triacylglycerols.高分辨率核磁共振光谱法——在脂肪酸和三酰甘油中的应用
Lipids. 1997 Oct;32(10):1019-34. doi: 10.1007/s11745-997-0132-y.
Lipids. 2002 Jan;37(1):111-6. doi: 10.1007/s11745-002-0870-x.