Gerkin RE
Department of Chemistry, The Ohio State University, Columbus, Ohio 43210, USA.
Acta Crystallogr C. 2000 Oct;56 (Pt 10):1218-9. doi: 10.1107/s0108270100007629.
The title compound, C(11)H(15)NO(2), crystallized in the centrosymmetric space group P2(1)/n with one molecule in the asymmetric unit. There is a single intermolecular hydrogen bond, in which the N(donor).O(acceptor) distance is 3.0374 (11) A and the N-H. O angle is 171.0 (12) degrees. The single intramolecular hydrogen bond has an O(donor).O(acceptor) distance of 2.6279 (11) A and an O-H.O angle of 161.8 (14) degrees. The four leading intermolecular C-H.O interactions have H.O distances ranging from 2.52 to 2.65 (2) A and C-H.O angles ranging from 125.2 (9) to 143 degrees. Chains of interactions form two-dimensional networks.
标题化合物C(11)H(15)NO(2)结晶于中心对称空间群P2(1)/n中，不对称单元中有一个分子。存在一个单一的分子间氢键，其中N（供体）.O（受体）距离为3.0374(11) Å，N-H.O角度为171.0(12)度。单一的分子内氢键的O（供体）.O（受体）距离为2.6279(11) Å，O-H.O角度为161.8(14)度。四个主要的分子间C-H.O相互作用的H.O距离在2.52至2.65(2) Å之间，C-H.O角度在125.2(9)至143度之间。相互作用链形成二维网络。
