Unusual C-H small middle dot small middle dot small middle dotSe=C Interactions in Aldols of Chiral N-Acyl Selones Detected by Gradient-Selected (1)H-(77)Se HMQC NMR Spectroscopy and X-ray Crystallography This work was supported by the Los Alamos National Laboratory Directed Research and Development Fund (grant XAB2). We thank Dr. Judith Gallucci (Department of Chemistry, Ohio State University) for obtaining the X-ray structures of 1 and 3, and Dr. Charles Campana (Bruker Analytical X-ray Systems in Madison, WI) for obtaining the X-ray structure of 2.

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作者信息

Michalczyk R, Schmidt JG, Moody E, Li Z, Wu R, Dunlap RB, Odom JD, Silks III

机构信息

Bioscience Division, The Leo Szilard Resource Los Alamos National Laboratory, MS E529 Los Alamos, NM, 87545 (USA).

出版信息

Angew Chem Int Ed Engl. 2000 Sep 1;39(17):3067-3070.

PMID:11028033

Abstract

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相似文献

Unusual C-H small middle dot small middle dot small middle dotSe=C Interactions in Aldols of Chiral N-Acyl Selones Detected by Gradient-Selected (1)H-(77)Se HMQC NMR Spectroscopy and X-ray Crystallography This work was supported by the Los Alamos National Laboratory Directed Research and Development Fund (grant XAB2). We thank Dr. Judith Gallucci (Department of Chemistry, Ohio State University) for obtaining the X-ray structures of 1 and 3, and Dr. Charles Campana (Bruker Analytical X-ray Systems in Madison, WI) for obtaining the X-ray structure of 2.

Angew Chem Int Ed Engl. 2000 Sep 1;39(17):3067-3070.

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