Wu D H, He C, Duan C Y, You X Z
Coordination Chemistry Institute & State Key Laboratory of Coordination Chemistry, Nanjing University, Nanjing 210093, People's Republic of China.
Acta Crystallogr C. 2000 Nov;56 Pt 11:1336-7. doi: 10.1107/s0108270100009914.
The thiosemicarbazone molecule in C(10)H(12)N(6)S(2).2C(3)H(7)NO has -1 symmetry. The thiosemicarbazone moiety and the benzene ring are essentially coplanar, with mean and maximum deviations of 0.03 and 0. 11 A, respectively. The dimethylformamide molecules bridge the thiosemicarbazone moieties, forming two-dimensional sheets through N-H.O hydrogen bonds.
C(10)H(12)N(6)S(2).2C(3)H(7)NO中的硫代半卡巴腙分子具有-1对称性。硫代半卡巴腙部分和苯环基本共面,平均偏差和最大偏差分别为0.03 Å和0.11 Å。二甲基甲酰胺分子连接硫代半卡巴腙部分,通过N-H.O氢键形成二维片层。