López-Mesas M, Crespi M, Brach J, Mullender J P
Laboratorio de Control de la Contaminación Ambiental, Instituto de Investigación Textil y Cooperación Industrial, Terrassa, Spain.
J Chromatogr Sci. 2000 Dec;38(12):551-5. doi: 10.1093/chromsci/38.12.551.
In this study, the efficiency of a clean-up method by gel permeation chromatography (GPC) for the separation of pesticides from lanolin is analyzed. The pesticides analyzed belong to two different families, organophosphorous and synthetic pyrethroids. Lanolin, a standard mixture of the pesticides, and a lanolin-pesticides mixture are injected in a GPC column. The recoveries and elution times from the GPC column of lanolin (by a gravimetric method) and pesticides (by gas chromatography-electron capture detector) are determined. From this column, a good separation of the lanolin-pesticides mixture is observed.
在本研究中,分析了凝胶渗透色谱法(GPC)从羊毛脂中分离农药的净化方法的效率。所分析的农药属于两个不同的类别,有机磷类和合成拟除虫菊酯类。将羊毛脂、农药标准混合物以及羊毛脂 - 农药混合物注入GPC柱。通过重量法测定羊毛脂从GPC柱的回收率和洗脱时间,通过气相色谱 - 电子捕获检测器测定农药的回收率和洗脱时间。从该柱中,可以观察到羊毛脂 - 农药混合物得到了良好的分离。