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食品模拟液对复合树脂和聚酸改性复合树脂修复材料弯曲强度的影响。

Effect of food-simulating liquids on the flexural strength of composite and polyacid-modified composite restoratives.

作者信息

Yap A U, Tan D T, Goh B K, Kuah H G, Goh M

机构信息

National University of Singapore, 5 Lower Kent Ridge Road, Singapore 119074, Republic of Singapore.

出版信息

Oper Dent. 2000 May-Jun;25(3):202-8.

Abstract

This study investigates the effects of food-simulating liquids on composite and polyacid-modified composite restoratives. Three composite (Z100, Spectrum TPH, and Tetric Ceram) and three polyacid-modified composite (F2000, Dyract AP, and Compoglass) restoratives from the same manufacturers were selected for the study. Flexural strength specimens (25 x 2 x 2 mm) based on ISO 4049 specifications were fabricated according to the manufacturers recommendations. After light polymerization, the specimens were removed from their molds and conditioned for one week at 37 degrees C in the following mediums: (1) deionized water, (2) 0.02 M citric acid, (3) heptane, and (4) 50% ethanol-water solution. Specimens stored in air were used as controls. The sample size was five for each material-medium combination. After conditioning, the specimens were blotted dry, measured, and subjected to flexural strength testing using an Instron Universal Testing Machine with a crosshead speed of 0.05 mm/minute. With the exception of Compoglass, flexural strength of all restoratives after conditioning in heptane was significantly greater than that after conditioning in all other mediums and the control. Although no significant difference in flexural strength values was observed between the different restoratives when the materials were conditioned in heptane or air (control), significant differences were observed between the different restoratives after conditioning in aqueous solutions (water, citric acid, and ethanol-water solution). The flexural strengths of the composites were generally significantly higher than their polyacid-modified counterparts after conditioning in the various aqueous solutions. The detrimental effects of aqueous solutions on flexural strength appeared to be greater with polyacid-modified composite resins than with composite restoratives.

摘要

本研究调查了食品模拟液对复合树脂和聚酸改性复合树脂修复材料的影响。从同一制造商处选取了三种复合树脂(Z100、Spectrum TPH和Tetric Ceram)和三种聚酸改性复合树脂(F2000、Dyract AP和Compoglass)修复材料用于该研究。根据ISO 4049规范制作弯曲强度试样(25×2×2毫米),并按照制造商的建议进行操作。光固化后,将试样从模具中取出,并在37摄氏度的以下介质中放置一周进行老化处理:(1)去离子水,(2)0.02M柠檬酸,(3)庚烷,以及(4)50%乙醇水溶液。储存在空气中的试样用作对照。每种材料 - 介质组合的样本量为五个。老化处理后,将试样吸干、测量,并使用Instron万能材料试验机以0.05毫米/分钟的十字头速度进行弯曲强度测试。除Compoglass外,所有修复材料在庚烷中老化后的弯曲强度均显著高于在所有其他介质及对照中的弯曲强度。尽管在庚烷或空气中(对照)老化处理时,不同修复材料的弯曲强度值未观察到显著差异,但在水溶液(水、柠檬酸和乙醇水溶液)中老化处理后,不同修复材料之间观察到了显著差异。在各种水溶液中老化处理后,复合树脂的弯曲强度通常显著高于其聚酸改性对应物。聚酸改性复合树脂在水溶液中对弯曲强度的有害影响似乎比复合树脂修复材料更大。

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