Wu H., Inkson B. J., Roberts S. G.
Department of Materials, University of Oxford, Oxford, UK.
J Microsc. 2001 Feb;201(2):212-220. doi: 10.1046/j.1365-2818.2001.00768.x.
Under machine grinding, material removal in monolithic Al2O3 is by intergranular fracture and grain pull-out. In comparison, under the same grinding conditions, an Al2O3/5%SiC nanocomposite undergoes significant surface grooving and intragranular fracture. The subsurface deformation mechanisms were investigated by cross-sectional transmission electron microscopy. For Al2O3, the residual deformation zone was localized very close to the surface in the first layer of grains, with dislocations occurring only within 1.5 µm of the top surface and a high density of basal twins penetrating to a depth of one single grain. Cracks were present along grain boundaries or basal twin interfaces. For Al2O3/SiC nanocomposites, the main residual plastic deformation is observed to be dislocations activated to a depth of about 10 µm (approx. 3-4 grains), with twinning rarely observed. Possible mechanisms by which the SiC particles influence the subsurface deformation and material removal modes are discussed.
在机械磨削过程中,整块Al2O3的材料去除是通过沿晶断裂和晶粒拔出实现的。相比之下,在相同的磨削条件下,Al2O3/5%SiC纳米复合材料会出现明显的表面沟槽和穿晶断裂。通过横截面透射电子显微镜研究了亚表面变形机制。对于Al2O3,残余变形区非常靠近表面的第一层晶粒,位错仅出现在顶面以下1.5 µm范围内,并且高密度的基面孪晶穿透到单个晶粒深度。沿晶界或基面孪晶界面存在裂纹。对于Al2O3/SiC纳米复合材料,主要的残余塑性变形被观察到位错激活深度约为10 µm(约3-4个晶粒),很少观察到孪晶。讨论了SiC颗粒影响亚表面变形和材料去除模式的可能机制。