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Nitroglycal Concatenation: A Broadly Applicable and Efficient Approach to the Synthesis of Complex O-Glycans This work was supported by the Deutsche Forschungsgemeinschaft and the European Community (grant no. FAIR-CT 97-3142). G.A.W. gratefully acknowledges a RIKEN/Studienstiftung des Deutschen Volkes fellowship. We are grateful to Dr. A. Geyer for his help in the structural assignments by NMR experiments and to Dr. K.-H. Jung for his help in the preparation of the manuscript.

作者信息

Winterfeld Gottfried A., Schmidt Richard R.

机构信息

Fachbereich Chemie, Universität Konstanz, Fach M 725 78457 Konstanz (Germany).

出版信息

Angew Chem Int Ed Engl. 2001 Jul 16;40(14):2654-2657.

PMID:11458362
Abstract
摘要

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1
Nitroglycal Concatenation: A Broadly Applicable and Efficient Approach to the Synthesis of Complex O-Glycans This work was supported by the Deutsche Forschungsgemeinschaft and the European Community (grant no. FAIR-CT 97-3142). G.A.W. gratefully acknowledges a RIKEN/Studienstiftung des Deutschen Volkes fellowship. We are grateful to Dr. A. Geyer for his help in the structural assignments by NMR experiments and to Dr. K.-H. Jung for his help in the preparation of the manuscript.硝酸甘油串联：一种广泛适用且高效合成复杂O-聚糖的方法 本研究得到了德国研究基金会和欧洲共同体（资助号：FAIR-CT 97-3142）的支持。G.A.W. 衷心感谢日本理化学研究所/德国人民学习基金会提供的奖学金。我们感谢A. Geyer博士在通过核磁共振实验进行结构归属方面提供的帮助，以及K.-H. Jung博士在稿件撰写方面提供的帮助。
Angew Chem Int Ed Engl. 2001 Jul 16;40(14):2654-2657.
2
1H High-Resolution Magic Angle Spinning NMR Spectroscopy for the Investigation of a Ras Lipopeptide in a Lipid Membrane This work was supported by the Deutsche Forschungsgemeinschaft (SFB 197 and Innovationskolleg "Chemisches Signal und biologische Antwort"). D.H. is grateful for a BASF fellowship through the Studienstiftung des Deutschen Volkes. The authors thank Dr. A. Pampel for technical support with the DRX600.
Angew Chem Int Ed Engl. 2001 Mar 16;40(6):1056-1058. doi: 10.1002/1521-3773(20010316)40:6<1056::aid-anie10560>3.0.co;2-7.
3
Structure and Dynamics of the Host-Guest Complex of a Molecular Tweezer: Coupling Synthesis, Solid-State NMR, and Quantum-Chemical Calculations S.P.B. thanks the Alexander von Humboldt Foundation for a research fellowship. C.O. acknowledges financial support by a Liebig "Habilitation" fellowship from the Fonds der Chemischen Industrie (FCI). This work was supported by the Deutsche Forschungsgemeinschaft (SFB 452) and the FCI. We thank Dr. Ingo Schnell for his involvement in the early part of this project, Dr. Kay Saalwächter for advice concerning the heteronuclear experiment, and Dr. Ulrich Burkert for his help during the synthesis of the complex.分子镊子主客体复合物的结构与动力学：耦合合成、固态核磁共振及量子化学计算 S.P.B. 感谢亚历山大·冯·洪堡基金会授予的研究奖学金。C.O. 感谢化学工业基金会（FCI）的利比希“教授资格”奖学金提供的资金支持。本研究得到了德国研究基金会（SFB 452）和 FCI 的支持。我们感谢英戈·施内尔博士参与本项目早期工作，感谢凯·萨尔瓦赫特博士在异核实验方面提供的建议，以及乌尔里希·布尔克特博士在复合物合成过程中给予的帮助。
Angew Chem Int Ed Engl. 2001 Feb 16;40(4):717-720.
4
Synthesis of Functionalized Cyclohexadiene-trans-Diols with Recombinant Cells of Escherichia coli D.F. was financially supported by the Graduiertenförderung des Landes NRW and the Studienstiftung des deutschen Volkes. We thank Professor Dr. Klaus Hantke, Universität Tübingen, for kindly providing the E. coli mutants H1882 and AN193. We thank Professor Dr. Eckhard Leistner, Universität Bonn, and Dr. Rolf Müller, GBF Braunschweig, for helpful discussions. Skillful technical assistance of Mrs. Ursula Degner and Ms. Regine Halbach is gratefully acknowledged. We thank Professor Dr. Christian Wandrey for his continuous and generous support.利用大肠杆菌D.F. 的重组细胞合成功能化环己二烯-反式二醇得到了北莱茵-威斯特法伦州的研究生资助以及德国人民学习基金会的资金支持。我们感谢图宾根大学的克劳斯·汉特克教授博士，他友好地提供了大肠杆菌突变体H1882和AN193。我们感谢波恩大学的埃克哈德·莱斯特纳教授博士以及布伦瑞克亥姆霍兹分子生物医学研究中心的罗尔夫·米勒博士给予的有益讨论。衷心感谢乌苏拉·德格纳夫人和雷吉娜·哈尔巴赫女士提供的专业技术协助。我们感谢克里斯蒂安·万德里教授博士给予的持续且慷慨的支持。
Angew Chem Int Ed Engl. 2001 Feb 2;40(3):555-557.
5
A Homoleptic Carbene--Lithium Complex Homoleptic carbene complexes part 10. This work was supported by the Fonds der Chemischen Industrie, the Deutsche Forschungsgemeinschaft, and by the Studienstiftung des Deutschen Volkes. Part 9 ref. 14.一种均配型卡宾-锂配合物 均配型卡宾配合物第10部分。本研究得到了化学工业基金会、德国研究基金会以及德意志学术交流中心的支持。第9部分参考文献14。
Angew Chem Int Ed Engl. 2001 May 18;40(10):1907-1910. doi: 10.1002/1521-3773(20010518)40:10<1907::aid-anie1907>3.0.co;2-1.
6
Toward Fully Synthetic Homogeneous Glycoproteins: A High Mannose Core Containing Glycopeptide Carrying Full H-Type 2 Human Blood Group Specificity This work was supported by the National Institutes of Health (Grant nos.: HL-25848 and CA-28824 (to S.J.D.), and CA-710506 (to K.O.L.)). Postdoctoral fellowship support is gratefully acknowledged by Z.-G.W. (US Army breast cancer grant no.: DAMD17-97-1-7119) and M.V. (NIH grant no.: CA-62948-04). We gratefully acknowledge Dr. George Sukenick of the Sloan-Kettering Institute's NMR core facility for mass spectral and NMR spectroscopic analyses (SKI core grant no.: CA-08748).
Angew Chem Int Ed Engl. 2001 May 4;40(9):1728-1732.
7
Thwarting beta-Hydride Elimination: Capture of the Alkylpalladium Intermediate of an Asymmetric Intramolecular Heck Reaction This research was supported by the National Institutes of Health (grant GM-12389). M.O. thanks the Deutsche Forschungsgemeinschaft (DFG) for an Emmy Noether fellowship (Oe 249/1-1). NMR and mass spectra were determined at the University of California, Irvine with instruments purchased with the assistance of the NSF and NIH shared instrumentation programs. We are grateful to Dr. Joseph W. Ziller and Dr. John Greaves for their assistance with X-ray structure and mass spectrometric analyses.
Angew Chem Int Ed Engl. 2001 Apr 17;40(8):1439-1442.
8
Application of a Planar Chiral eta(5)-Cyclopentadienylrhenium(I)tricarbonyl Complex in Asymmetric Catalysis: Highly Enantioselective Phenyl Transfer to Aldehydes We are grateful to the Deutsche Forschungsgemeinschaft (DFG) within the Collaborative Research Center (SFB) 380 "Asymmetric Synthesis by Chemical and Biological Methods" and the Fonds der Chemischen Industrie for financial support and to Dr. C. W. Lehmann, MPI für Kohlenforschung, Mülheim, for collecting the X-ray diffraction data. M.K. acknowledges the DFG for a predoctoral fellowship (Graduiertenkolleg). We thank Degussa and Witco for donations of chemicals and Professor Dr. A. Salzer as well as Dipl.-Ing. M. Treu for inspiring discussions. We also appreciate the stimulus of Dr. K. Muñiz for the investigation of the influence of the metal-pi-fragment on catalyses of this type.
Angew Chem Int Ed Engl. 2001 Apr 17;40(8):1488-1490.
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P(6) Manganocene and P(3) Cymantrene: Consequences of the Inclusion of Phosphorus Atoms in Mn-Coordinated Cyclopentadienyl Ligands This work was supported by the Deutsche Forschungsgemeinschaft and the Fonds der Chemischen Industrie. A.E., M.H., and M.Z. thank the DFG-Graduiertenkolleg ("Phosphorchemie als Bindeglied verschiedener chemischer Disziplinen" of the University of Kaiserslautern) and M.Z. also thanks the Studienstiftung des Deutschen Volkes for fellowships.
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10
The Synthesis of CP-263,114 and CP-225,917: Striking Long-Range Stereocontrol in the Fashioning of C7 Financial support was provided by the National Institutes of Health (Grant nos. CA-28824 and HL-25848 for S.J.D., CA-08748 for the Sloan-Kettering Institute Core Facility). Q.T. gratefully acknowledges the US Department of Defense for a postdoctoral fellowship (U.S. Army grant no. DAMD-17-99-1-9373). We thank the Pfizer Corporation, particularly Dr. T. Kaneko and Dr. T. T. Dabrah for discussions and for providing valuable CP samples from fermentation broth. We are grateful to Dr. Dongfang Meng for his major contributions to this work. We also thank George Sukenick of the Sloan-Kettering Institute Core Facility for mass spectral analyses and assistance in NMR spectroscopic and HPLC analyses, and Sylvi Rusli for mass spectral analyses.CP - 263,114和CP - 225,917的合成：在构建C7时显著的远程立体控制 美国国立卫生研究院提供了资金支持（给S.J.D.的CA - 28824和HL - 25848号拨款，给斯隆 - 凯特琳研究所核心设施的CA - 08748号拨款）。Q.T.衷心感谢美国国防部授予的博士后奖学金（美国陆军拨款号DAMD - 17 - 99 - 1 - 9373）。我们感谢辉瑞公司，特别是T. Kaneko博士和T.T. Dabrah博士进行的讨论以及提供来自发酵液的宝贵CP样品。我们感谢董方孟博士对这项工作的重大贡献。我们还感谢斯隆 - 凯特琳研究所核心设施的George Sukenick进行质谱分析以及在核磁共振光谱分析和高效液相色谱分析方面提供的帮助，感谢Sylvi Rusli进行质谱分析。
Angew Chem Int Ed Engl. 2000 Dec 15;39(24):4509-4511.

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