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基于直接热解吸-气相色谱-嗅觉测定法和样品稀释分析的油基烧烤调味料的香气成分

Aroma components of an oil-based grill flavoring by direct thermal desorption-gas chromatography-olfactometry and sample dilution analysis.

作者信息

Webb T E, Cadwallader K R

机构信息

Department of Food Science and Technology, Mississippi Agricultural Experiment Station, Mississippi State University, USA.

出版信息

Adv Exp Med Biol. 2001;488:143-50. doi: 10.1007/978-1-4615-1247-9_12.

Abstract

Grill flavorings are a convenient way for food processors to impart grill-like flavor to meat products that have not been grilled. In this study a commercially available oil-based processed grill flavoring was analyzed by direct thermal desorption (DTD)-gas chromatography-olfactometry (GCO) and DTD-GC-mass spectrometry (MS). Sample mass dilution analysis-GCO was used to indicate which compounds had the greatest impact on the overall aroma of the sample. Major aroma contributors included 1-octen-3-one, 2-methoxyphenol, and (E)-2-nonenal. Minor contributors were (E)-2-decenal and 2,4-decadienal. Other major contributors, characterized as having grill aroma notes, were unidentified. Excluding the possibility of artifact formation from the thermal degradation of fatty acid hydroperoxides, DTD functioned well as a GCO technique, but poorly as a qualitative GC-MS technique.

摘要

烧烤调味料是食品加工商为未经过烧烤的肉制品赋予类似烧烤风味的便捷方式。在本研究中,采用直接热脱附(DTD)-气相色谱-嗅觉测定法(GCO)和DTD-气相色谱-质谱联用法(MS)对一种市售的油基加工烧烤调味料进行了分析。采用样品质量稀释分析-GCO来表明哪些化合物对样品的整体香气影响最大。主要的香气成分包括1-辛烯-3-酮、2-甲氧基苯酚和(E)-2-壬烯醛。次要成分是(E)-2-癸烯醛和2,4-癸二烯醛。其他具有烧烤香气特征的主要成分未明确。排除脂肪酸氢过氧化物热降解产生伪像的可能性后,DTD作为一种GCO技术效果良好,但作为一种定性GC-MS技术效果不佳。

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