Itoh T, Fukushima T, Inoue Y, Matsuo N, Matsumoto M
Department of Orthodontics, Fukuoka Dental College, Japan.
Am J Dent. 2000 Aug;13(4):181-6.
To examine the effect of contamination on the bond strength of orthodontic brackets cemented with either a commercial (Fuji Ortho LC) or an experimental light-cured glass-ionomer cement to enamel, and the effect of etching times on the bond strength.
MATERIALS & METHODS: Simulated metal brackets were applied with the cements to bond polished and etched (37% phosphoric acid) bovine enamel with and without contamination by water, human saliva, and blood. After 1-day water immersion, the shear bond strengths were measured. The fractured surfaces were examined using SEM. Additional tests were conducted on: (1) the Knoop hardness of the contaminated cements, (2) the HEMA composition of the cements, (3) the viscosity of the cements, and (4) the intensity of transmitted visible light through the contaminants. The results were compared by ANOVA and Duncan's tests at P=0.05.
Water and saliva reduced the bond strength to polished and etched enamel, except for the bond strength of Fuji Ortho LC to polished enamel. The blood contamination produced poor bond strengths to polished and etched enamel. The experimental cement showed higher bond strengths to polished enamel with water and saliva contamination than Fuji Ortho LC. The bond strength of the experimental cement to etched enamel with and without contamination were comparable to those of Fuji Ortho LC. SEM micrographs revealed that the specimens exhibiting high bond strengths to polished and etched enamel mainly had cement-enamel interface failure and cement-metal mesh interface failure, respectively. Fuji Ortho LC had higher HEMA concentration than the experimental cement. The highest viscosity was measured with blood, followed by saliva and water. Blood contamination, showing the highest attenuation of the light intensity, reduced Knoop hardness of the experimental cement and Fuji Ortho LC.
研究污染对用市售(Fuji Ortho LC)或实验性光固化玻璃离子水门汀粘结至牙釉质的正畸托槽粘结强度的影响,以及酸蚀时间对粘结强度的影响。
将模拟金属托槽用这些水门汀粘结至经抛光和酸蚀(37%磷酸)的牛牙釉质,分为有水、人唾液和血液污染组与无污染组。水浸1天后,测量剪切粘结强度。使用扫描电子显微镜检查断裂面。还进行了以下额外测试:(1)污染水门汀的努氏硬度;(2)水门汀的甲基丙烯酸羟乙酯(HEMA)组成;(3)水门汀的粘度;(4)污染物对可见光的透射强度。结果通过方差分析和Duncan检验进行比较,P = 0.05。
水和唾液降低了粘结至抛光和酸蚀牙釉质的粘结强度,但Fuji Ortho LC粘结至抛光牙釉质的粘结强度除外。血液污染导致粘结至抛光和酸蚀牙釉质的粘结强度较差。实验性水门汀在有水和唾液污染时粘结至抛光牙釉质的粘结强度高于Fuji Ortho LC。实验性水门汀粘结至有污染和无污染酸蚀牙釉质的粘结强度与Fuji Ortho LC相当。扫描电子显微镜照片显示,对抛光和酸蚀牙釉质表现出高粘结强度的标本分别主要发生水门汀 - 牙釉质界面破坏和水门汀 - 金属网界面破坏。Fuji Ortho LC的HEMA浓度高于实验性水门汀。血液的粘度最高,其次是唾液和水。血液污染导致实验性水门汀和Fuji Ortho LC的努氏硬度降低,且光强度衰减最高。