通过D-葡萄糖酸-1,5-内酯硅烷化反应形成的四-O-（叔丁基二甲基硅基）-D-葡萄糖酸-1,4-内酯结构的确证。
Confirmation of the structure of tetra-O-(tert-butyldimethylsilyl)-D-glucono-1,4-lactone formed by silylation of D-glucono-1,5-lactone.
作者信息
Singh Janak, DiMarco John, Kissick Thomas P, Deshpande Prashant, Gougoutas Jack Z
机构信息
Process Research and Development, Bristol-Myers Squibb Pharmaceutical Research Institute, Princeton, NJ 08543, USA.
出版信息
Carbohydr Res. 2002 Mar 15;337(6):565-8. doi: 10.1016/s0008-6215(02)00014-9.
Abstract
The structure of tetra-O-(tert-butyldimethylsilyl)-D-glucono-1,4-lactone made by the silylation of D-glucono-1,5-lactone has been confirmed by single-crystal X-ray analysis.
摘要
通过单晶X射线分析确定了由D-葡萄糖酸-1,5-内酯硅烷化制备的四-O-（叔丁基二甲基甲硅烷基）-D-葡萄糖酸-1,4-内酯的结构。
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