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悬铃木叶八角枫苷D-J：来自日本八角枫（Alangium platanifolium (Sieb. et Zucc.) Harms var. platanifolium Sieb. et Zucc.）叶片的巨大戟烷糖苷

Platanionosides D-J: megastigmane glycosides from the leaves of Alangium platanifolium (Sieb. et Zucc.) Harms var. platanifolium Sieb. et Zucc.

作者信息

Otsuka Hideaki, Tamaki Akie

机构信息

Institute of Pharmaceutical Sciences, Hiroshima University Faculty of Medicine, Japan.

出版信息

Chem Pharm Bull (Tokyo). 2002 Mar;50(3):390-4. doi: 10.1248/cpb.50.390.

DOI:10.1248/cpb.50.390
PMID:11911204
Abstract

From the leaves of Alangium paltanifolium var. platanifolium, collected in Fukuoka Prefecture, twelve further megastigmane glycosides were isolated. Seven of them, named platanionosides D-J (1-7), were found to be new compounds. Their structures were elucidated from spectroscopic evidence and their absolute structures were determined from beta-D-glucosylation-induced shift trends of 13C-NMR and by application of a modified Mosher's method.

摘要

从采自福冈县的宽叶八角枫（Alangium paltanifolium var. platanifolium）叶片中，又分离出了12种巨大戟烷型糖苷。其中7种被命名为八角枫苷D-J（1-7），发现它们是新化合物。通过光谱数据阐明了它们的结构，并根据β-D-葡萄糖基化诱导的13C-NMR位移趋势以及应用改良的莫舍尔方法确定了它们的绝对构型。

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