Petukhov A V, Aarts D G A L, Dolbnya I P, De Hoog E H A, Kassapidou K, Vroege G J, Bras W, Lekkerkerker H N W
van 't Hoff Laboratory for Physical and Colloid Chemistry, Debye Institute, University of Utrecht, Padualaan 8, 3508 TB Utrecht, The Netherlands.
Phys Rev Lett. 2002 May 20;88(20):208301. doi: 10.1103/PhysRevLett.88.208301. Epub 2002 Apr 30.
The long-range order parameters in single crystals of hard colloidal spheres grown in sediments of colloid-polymer mixtures are determined using synchrotron small-angle x-ray diffraction with a resolution of 10(-6) of the wave vector. The interplanar positional order derived from the width of lattice reflections extends over at least 500 lattice planes. The lattice planes are orientationally correlated within approximately 0.1 degrees throughout the crystals, whereas the stacking of hexagonal planes remains random.