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[生物污渍中苯丙胺衍生物的筛查与检测]

[Screening and detection of amphetamine derivatives in biological stains].

作者信息

Schütz Harald, Gotta Jan Christoph, Erdmann Freidoon, Weiler Günter

机构信息

Institut für Rechtsmedizin, Universität Giessen.

出版信息

Arch Kriminol. 2002 Jul-Aug;210(1-2):22-7.

Abstract

A GC/MS-method is described for the screening, detection and determination of the commonly used drugs amphetamine, methamphetamine, MDA, MDMA and MBDB in small blood samples and bloodstains using solid phase SPE columns and a pipetting robot (Gilson Aspec XL). The detection limits are in the order of 0.03 to 0.08 microgram/L and the correlation factors between 0.9982 and 0.9998. Furthermore the stability was investigated covering a storage time of 64 days. The method has proven useful in forensic cases with only small sample volumes or bloodstains.

摘要

描述了一种气相色谱/质谱法,用于使用固相萃取柱和移液机器人(吉尔森Aspec XL)对小血样和血迹中的常用药物苯丙胺、甲基苯丙胺、MDA、摇头丸和MBDB进行筛查、检测和测定。检测限在0.03至0.08微克/升范围内,相关系数在0.9982至0.9998之间。此外,还研究了长达64天储存时间的稳定性。该方法已证明在样本量小或仅有血迹的法医案件中很有用。

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