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用阳极溶出伏安法对血液、尿液和骨骼中的铅进行定量测定（作者译）

[Quantitative determination of lead in blood, urine and bone by anodic stripping voltammetry (author's transl)].

作者信息

Kisser W

出版信息

Arch Toxicol. 1975 Nov 20;34(3):237-41. doi: 10.1007/BF00353286.

DOI:10.1007/BF00353286
PMID:1243623
Abstract

The determination of lead in blood, urine and bone (0.5 to 1.0 g blood, 5 to 10 ml urine, approx. 200 mg bone ash) by anodic stripping voltammetry is described. Blood samples are decomposed with nitric acid/perchloric acid, urine samples with nitric acid/perchloric acid/sulfuric acid. Bones are dry-ashed at 450 to 500 degrees C previously. The interference of iron in the analysis of blood samples is removed by adding citrate and adjusting the pH to approx. 3.5.

摘要

本文描述了采用阳极溶出伏安法测定血液、尿液和骨骼（0.5至1.0克血液、5至10毫升尿液、约200毫克骨灰）中的铅。血液样本用硝酸/高氯酸分解，尿液样本用硝酸/高氯酸/硫酸分解。骨骼预先在450至500摄氏度下进行干灰化。通过加入柠檬酸盐并将pH值调节至约3.5来消除血液样本分析中铁的干扰。

相似文献

1
[Quantitative determination of lead in blood, urine and bone by anodic stripping voltammetry (author's transl)].用阳极溶出伏安法对血液、尿液和骨骼中的铅进行定量测定（作者译）
Arch Toxicol. 1975 Nov 20;34(3):237-41. doi: 10.1007/BF00353286.
2
Application of pulse polarography with anodic stripping voltammetry to biological and toxicological analyses for lead and cadmium.脉冲极谱法结合阳极溶出伏安法在铅和镉的生物及毒理学分析中的应用。
Pathol Biol (Paris). 1975 May;23(5):379-86.
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Determination of lead in blood and urine by anodic stripping voltammetry.
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Studies on the determination of blood lead by neopolarographic anodic stripping voltammetry.新极谱阳极溶出伏安法测定血铅的研究。
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Dry ash-voltammetric determination of cadmium, cooper, lead, and zinc in foods.食品中镉、铜、铅和锌的干灰化伏安法测定
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[Lead detection and measurement in biological fluids by means of anodic stripping voltammetry (author's transl)].通过阳极溶出伏安法对生物流体中的铅进行检测和测量（作者译）
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Rapid micromethod for blood lead analysis by anodic stripping voltammetry.阳极溶出伏安法快速微量血铅分析法
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本文引用的文献

1
[On normal lead content in human bone].[关于人体骨骼中的正常铅含量]
Arch Toxikol. 1961;19:34-48.
2
Use of the mercury drop electrode method for direct evaluation of minute amounts of lead in urine.使用汞滴电极法直接评估尿液中的微量铅。
Nature. 1961 Jan 7;189:57-8. doi: 10.1038/189057a0.
3
[On the quantitative mass spectrometry of the normal thallium content in the human organism].
Arch Toxikol. 1967;22(4):255-74.
4
[Determination of lead, copper, thallium, bismuth, and zinc in blood serum by the method of anodic stripping-polarography].阳极溶出极谱法测定血清中的铅、铜、铊、铋和锌
Mikrochim Acta. 1972(2):163-72.
5
[The methodology of polarographic lead determination in urine and blood].[尿液和血液中铅的极谱测定方法]
Mikrochim Acta. 1974(3):545-8.