米尔斯等人测定食品中农药残留方法扩展的合作研究。
Collaborative study of an extension of the Mills et al. method for the determination of pesticide residues in foods.
作者信息
Finsterwalder C E
出版信息
J Assoc Off Anal Chem. 1976 Jan;59(1):169-71.
Fifteen laboratories collaboratively determined parathion, o,p'-DDT, p,p'-DDT, and p,p'-DDE in kale, and lindane, dieldrin, heptachlor epoxide, and p,p'-DDE in eggs, using electron capture gas-liquid chromatography (potassium chloride thermionic detector for parathion). Pesticide levels ranged from 0.033 ppm heptachlor epoxide to 3.32 ppm p,p'-DDT. Mean recoveries (+/- standard deviations) were: parathion 91+/-15%, o,p'-DDT 99+/-8%, P,P'-DDT 97+/-8%, lindane 94+/-4%, dieldrin 106+/-8%, heptachloro epoxide 106+/-5%, p,p'-DDE 94+/-8% in eggs and 101+/-9% in kale. The methods have been adopted as official first action.
十五个实验室合作，使用电子捕获气液色谱法（对硫磷用氯化钾热离子检测器）测定了羽衣甘蓝中的对硫磷、o,p'-滴滴涕、p,p'-滴滴涕和p,p'-滴滴伊，以及鸡蛋中的林丹、狄氏剂、环氧七氯和p,p'-滴滴伊。农药含量范围从环氧七氯的0.033 ppm到p,p'-滴滴涕的3.32 ppm。平均回收率（±标准偏差）为：鸡蛋中对硫磷91±15%、o,p'-滴滴涕99±8%、p,p'-滴滴涕97±8%、林丹94±4%、狄氏剂106±8%、环氧七氯106±5%、p,p'-滴滴伊94±8%，羽衣甘蓝中p,p'-滴滴伊为101±9%。这些方法已被采用为官方首次行动方法。
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