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添加聚甲基丙烯酸甲酯纤维对高强度热固化丙烯酸树脂义齿基托材料某些性能的影响。

The effect of the addition of poly(methyl methacrylate) fibres on some properties of high strength heat-cured acrylic resin denture base material.

作者信息

Jagger D, Harrison A, Jagger R, Milward P

机构信息

Department of Oral and Dental Science, Bristol Dental School, University of Bristol, Bristol, UK.

出版信息

J Oral Rehabil. 2003 Mar;30(3):231-5. doi: 10.1046/j.1365-2842.2003.01011.x.

Abstract

The self-reinforcement of acrylic resin with butadiene styrene surface treated poly(methyl methacrylate) fibres has been reported to have the potential to substantially improve the transverse bend strength of conventional heat-cured acrylic resin. The aim of this study was to investigate the effect of the addition of butadiene styrene surface treated poly(methyl methacrylate) fibres in cross-ply arrangement to high impact acrylic resin on the transverse and impact strength. Specimens were prepared as specified in the International Standard Organization and British Standards for the Testing of Denture Base Resins (ISO 1567, 1988; BS 2487, 1989) and the British Standard Specification for Orthodontic resins (BS 6747, 1987) for transverse bend and impact testing. The impact strength was measured using a Zwick pendulum impact tester and the transverse bend strength measured using a Lloyds Instruments testing machine. The results showed that the impact strength was not improved with the addition of fibres, high impact acrylic resin with fibres (LF) 11.1 kJ m-2 and high impact acrylic resin (L) (12.5 kJ m-2). The modulus of rupture was decreased with the addition of fibres (57.8 MPa) for (LF) compared with (60.4 MPa) for (L). The modulus of elasticity was also reduced with the addition of fibres (1834.9 MPa) (LF) and 2086.2 MPa (L) as was the peak load (LF) (50.8 N) and (L) (55.8 N). It was concluded that the addition of surface treated poly(methyl methacrylate) fibres in cross-ply arrangement to high strength acrylic resin did not produce an improvement in the impact or transverse strength and cannot be recommended as a method of reinforcement.

摘要

据报道,用丁苯橡胶表面处理的聚甲基丙烯酸甲酯纤维对丙烯酸树脂进行自增强,有可能显著提高传统热固化丙烯酸树脂的横向弯曲强度。本研究的目的是探讨以交叉铺层排列方式添加丁苯橡胶表面处理的聚甲基丙烯酸甲酯纤维对高抗冲丙烯酸树脂横向强度和抗冲击强度的影响。按照国际标准组织和英国假牙基托树脂测试标准(ISO 1567, 1988;BS 2487, 1989)以及英国正畸树脂标准规范(BS 6747, 1987)制备试样,用于横向弯曲和抗冲击测试。使用Zwick摆锤式冲击试验机测量抗冲击强度,使用Lloyds Instruments试验机测量横向弯曲强度。结果表明,添加纤维后抗冲击强度并未提高,含纤维的高抗冲丙烯酸树脂(LF)为11.1 kJ m-2,高抗冲丙烯酸树脂(L)为12.5 kJ m-2。与(L)的60.4 MPa相比,添加纤维后的(LF)的断裂模量降低(57.8 MPa)。添加纤维后,弹性模量也降低了,(LF)为1834.9 MPa,(L)为2086.2 MPa,峰值载荷(LF)为50.8 N,(L)为55.8 N。得出的结论是,以交叉铺层排列方式向高强度丙烯酸树脂中添加表面处理的聚甲基丙烯酸甲酯纤维并不能提高抗冲击强度或横向强度,因此不能推荐将其作为一种增强方法。

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