Hoben H J, Ching S A, Casarett L J, Young R A
Bull Environ Contam Toxicol. 1976 Jan;15(1):78-85. doi: 10.1007/BF01686198.
Simple and flexible methods have been designed for the determination of pentachlorophenol in animal tissue, blood plasma, urine, and aerosol. The isolation of the pesticide is achieved through its extraction with benzene or hexane after acidification, derivatization, and its subsequent purification through florosil columns. A brief describption of the sampling methods is included. The described procedures are especially suited for exposure experiments where different types of samples with a large variety of PCP concentrations are encountered.
已设计出简单灵活的方法来测定动物组织、血浆、尿液和气溶胶中的五氯苯酚。通过在酸化、衍生化后用苯或己烷萃取该农药，并随后通过弗罗里硅土柱进行纯化来实现其分离。文中包含了对采样方法的简要描述。所描述的程序特别适用于遇到不同类型且五氯苯酚浓度差异很大的样品的暴露实验。
