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[2,6-Bis(1H-benzimidazol-2-yl-kappaN3)pyridine-kappaN](dimethylformamide-kappaO)(thiosulfato-kappa2O,S)nickel(II) monohydrate.

作者信息

Freire Eleonora, Baggio Sergio, Muñoz Juan Carlos, Baggio Ricardo

机构信息

Universidad Nacional de la Patagonia, Sede Puerto Madryn, and CenPat, CONICET, 9120 Puerto Madryn, Chubut, Argentina.

出版信息

Acta Crystallogr C. 2003 Aug;59(Pt 8):m299-301. doi: 10.1107/s0108270103008667. Epub 2003 Jul 12.

DOI:10.1107/s0108270103008667
PMID:12909748
Abstract

The structure of the title compound, [Ni(ths)(bbip)(dmf)].H(2)O [ths is thiosulfate, S(2)O(3); bbip is 2,6-bis(1H-benzimidazol-2-yl)pyridine, C(21)H(13)N(5); and dmf is dimethylformamide, C(3)H(7)NO], is monomeric, with the nickel ion octahedrally surrounded by an N,N',N"-tridentate bbip molecule, an S,O-bidentate ths molecule and an O-monodentate dmf molecule. The H atoms of the hydration water molecule and the amino groups of bbip are involved in hydrogen bonding and determine a spatial organization of broad layers parallel to (001), which are connected by weak interactions.

摘要

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