[Synthesis and characterization of meso-tetra-(4-palmitoyloxyphenyl)porphyrin].

作者信息

An Q, Yang D, Shi T, Liu W

机构信息

Dept. of Material Science and Engineering, Dalian University of Technology, Dept. of Chemical Engineering, Dalian Institute of Light Industry, Dalian.

出版信息

Guang Pu Xue Yu Guang Pu Fen Xi. 2001 Aug;21(4):478-80.

PMID:12945266

Abstract

The meso-tetra-(4-palmitoyloxyphenyl)porphyrin(TPPPH2) was synthesized by esterification reaction with meso-tetra-(4-hydroxyphenyl)porphyrin(THPPH2) and Palmityl chloride as reactant. This product was separated and purified by column chromatography with silica gel as fixed phase and chloroform as washing agent, and characterized by means of elemental analysis, UV-visible spectrum, infrared photoacoustic spectrum and 1H NMR. The main spectra of UV, IR and 1H NMR were measured and investigated.

摘要