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Synthesis of lysine-containing fragments of the Proteus mirabilis O27 O-specific polysaccharide and neoglycoconjugates therefrom.

作者信息

Kononov L O, Krishna P R, Kochetkov N K, Rao A V

机构信息

N. D. Zelinsky Institute of Organic Chemistry, Academy of Sciences of the U.S.S.R., Moscow.

出版信息

Carbohydr Res. 1992 Mar 2;225(2):279-89. doi: 10.1016/s0008-6215(00)90501-9.

DOI:10.1016/s0008-6215(00)90501-9
PMID:1379517
Abstract

Amide-linked lysine mono- and di-uronic acid fragments of the O-specific polysaccharide from P. mirabilis O27 have been synthesised. N epsilon-Boc-L-lysine tert-butyl ester was condensed with 2-azidoethyl glycosides of glucuronic acid and beta-D-GlcpNAc-(1----3)-beta-D-GlcpA. Transformation of the products into 2-acrylamidoethyl glycosides, followed by deprotection using trifluoroacetic acid, gave the target monomers that were converted into high-molecular-weight copolymer-type neoglycoconjugates.

摘要

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