Attia Adel M E, El-Shehawy Ashraf A
Department of Chemistry, Faculty of Education, University of Tanta (Kafr El-Sheikh Branch), Tanta, Egypt.
Nucleosides Nucleotides Nucleic Acids. 2003 Sep;22(9):1737-46. doi: 10.1081/NCN-120023269.
Treatment of piperidinium salts of dihydropyridinethiolates 3 with glycosyl bromides 4 in dry acetone provides a convenient and high yielding synthesis of 1,4-dihydro-3-cyanopyridine thioglycosides 5. The structures of 5 were confirmed by oxidation as well as by 1H NMR and 13C NMR spectral analysis.
在干燥丙酮中，用糖基溴化物4处理二氢吡啶硫醇盐3的哌啶盐，可方便且高产率地合成1,4 - 二氢 - 3 - 氰基吡啶硫代糖苷5。5的结构通过氧化以及1H NMR和13C NMR光谱分析得以确证。
