Karacaer Ozgül, Polat Tülin N, Tezvergil Arzu, Lassila Lippo V J, Vallittu Pekka K
Department of Prosthodontics, Gazi University, Faculty of Dentistry, Turku, Finland.
J Prosthet Dent. 2003 Oct;90(4):385-93. doi: 10.1016/S0022391303005183.
Fiber-reinforcement has been used to overcome the mechanical limitations of denture base polymers. One major difficulty in the use of fiber reinforcement has been the addition of fibers during conventional processing methods.
This study evaluated the effect of various lengths and concentrations of chopped E-glass fiber-reinforcement on the transverse strength, modulus of elasticity, and impact strength of injection and compression-molded polymethyl methacrylate based denture base polymer.
Test specimens (n=10) of 4-, 6-, and 8-mm fiber length and 1%, 3%, and 5% weight fiber concentrations were prepared with either an injection or a compression-molded processing method. Denture base polymer specimens without any fiber reinforcement were used as control for both processing methods. Transverse strength test specimens (65 x 10 x 2.5 mm) were stored in water bath at 37 degrees C for 2 weeks. The transverse strength (MPa) and modulus of elasticity (GPa) was measured with the 3-point bending test. Impact strength (kJ/m(2)) test specimens (60 x 7.5 x 4 mm) were tested with the Charpy-type pendulum impact test setup. The data were analyzed with multifactorial analysis of variance and Tukey post hoc tests (alpha=.05).
Injection-molded fiber-reinforced groups showed significantly higher transversal strength, elastic modulus, and impact strength compared with compression-molded groups (P <.001). In the injection-molded groups, fiber concentration increased all mechanical properties tested (P <.05), but fiber length only increased transverse strength and modulus of elasticity (P <.05). In the compression molded groups, fiber concentration affected modulus of elasticity and impact strength significantly (P <.05), but fiber length did not show any significant effect on the mechanical properties tested (P >.05).
The transverse strength, elastic modulus and impact strength of injection-molded denture base polymer increased significantly with the use of chopped E-glass fibers, whereas the effect was not significant with the compression-molded polymer.
纤维增强材料已被用于克服义齿基托聚合物的机械性能局限。在传统加工方法中添加纤维存在一个主要困难。
本研究评估了不同长度和浓度的短切E玻璃纤维增强材料对注塑成型和模压成型的聚甲基丙烯酸甲酯基义齿基托聚合物的横向强度、弹性模量和冲击强度的影响。
采用注塑或模压成型加工方法制备纤维长度为4毫米、6毫米和8毫米以及纤维重量浓度为1%、3%和5%的测试样本(n = 10)。两种加工方法均使用未添加任何纤维增强材料的义齿基托聚合物样本作为对照。横向强度测试样本(65×10×2.5毫米)在37摄氏度的水浴中储存2周。采用三点弯曲试验测量横向强度(MPa)和弹性模量(GPa)。冲击强度(kJ/m²)测试样本(60×7.5×4毫米)采用夏比摆锤冲击试验装置进行测试。数据采用多因素方差分析和Tukey事后检验进行分析(α = 0.05)。
与模压成型组相比,注塑成型的纤维增强组的横向强度、弹性模量和冲击强度显著更高(P < 0.001)。在注塑成型组中,纤维浓度提高了所有测试的机械性能(P < 0.05),但纤维长度仅提高了横向强度和弹性模量(P < 0.05)。在模压成型组中,纤维浓度对弹性模量和冲击强度有显著影响(P < 0.05),但纤维长度对测试的机械性能没有显著影响(P > 0.05)。
使用短切E玻璃纤维可显著提高注塑成型义齿基托聚合物的横向强度、弹性模量和冲击强度,而对模压成型聚合物的影响不显著。