微波辅助多元醇法合成碲化铜铟（CuInTe2）和硒化铜铟（CuInSe2）纳米颗粒。
Microwave-assisted polyol synthesis of CuInTe2 and CuInSe2 nanoparticles.
作者信息
Grisaru Haviv, Palchik Oleg, Gedanken Aharon, Palchik Valery, Slifkin Michael A, Weiss Arie M
机构信息
Department of Chemistry, Bar-Ilan University, Ramat-Gan 52900, Israel.
出版信息
Inorg Chem. 2003 Nov 3;42(22):7148-55. doi: 10.1021/ic0342853.
Nanoparticles of the CuInTe(2) (CIT) and CuInSe(2) (CIS) alloys have been prepared using the microwave-assisted polyol method. In this simple and quick reaction the polyol is both the solvent and the reducing agent. XRD studies show that nanoparticles of CIT and CIS are formed in the body-centered tetragonal structure and their average diameters are approximately 94 and approximately 83 nm, respectively. Electron microscopy studies show that these formed particles are poorly aggregated with a mean diameter of 100 and 85 nm, respectively. The products have been characterized by different analytical techniques, and the electronic properties have been measured using photoacoustic spectroscopy (PAS).
采用微波辅助多元醇法制备了CuInTe₂（CIT）和CuInSe₂（CIS）合金的纳米颗粒。在这种简单快速的反应中，多元醇既是溶剂又是还原剂。X射线衍射研究表明，CIT和CIS纳米颗粒形成体心四方结构，其平均直径分别约为94 nm和约83 nm。电子显微镜研究表明，这些形成的颗粒聚集程度较低，平均直径分别为100 nm和85 nm。用不同的分析技术对产物进行了表征，并使用光声光谱（PAS）测量了其电子性质。
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