Mitra Sumita B, Wu Dong, Holmes Brian N
3M ESPE Dental Products, St. Paul, Minn. 55144, USA.
J Am Dent Assoc. 2003 Oct;134(10):1382-90. doi: 10.14219/jada.archive.2003.0054.
This article reports the authors' development of nanofillers and a resulting nanocomposite. They measured the nanocomposite's properties in vitro in comparison with those of several existing composites (hybrids, microhybrids and microfill).
The authors developed two types of nanofillers: nanomeric particles and nanoclusters. They used optimal combinations of these nanofillers in a proprietary resin matrix to prepare the nanocomposite system with a wide range of shades and opacities. The properties they studied were compressive, diametral tensile and flexural strengths; in vitro three-body wear; fracture resistance; polish retention; and surface morphology after toothbrush abrasion. They performed statistical analysis using analysis of variance/Tukey-Kramer paired analysis at a 95 percent confidence interval.
The compressive and diametral strengths and the fracture resistance of the nanocomposite were equivalent to or higher than those of the other commercial composites tested. The three-body wear results of the nanocomposite system were statistically better than those of all other composites tested. The nanocomposite showed better polish retention than the hybrids and microhybrids tested at the extended brushing periods. After extended toothbrush abrasion, the dentin, body and enamel shades showed polish retention equivalent to that of the microfill tested, while translucent shades showed better polish retention than the microfill.
The dental nanocomposite system studied showed high translucency, high polish and polish retention similar to those of microfills while maintaining physical properties and wear resistance equivalent to those of several hybrid composites.
The strength and esthetic properties of the resin-based nanocomposite tested should allow the clinician to use it for both anterior and posterior restorations.
本文报道了作者对纳米填料及由此产生的纳米复合材料的研发情况。他们在体外测量了该纳米复合材料的性能,并与几种现有复合材料(混合型、微混合型和微填料型)的性能进行了比较。
作者研发了两种类型的纳米填料:纳米颗粒和纳米团簇。他们在一种专利树脂基质中使用这些纳米填料的最佳组合,制备出具有广泛色泽和不透明度的纳米复合材料体系。他们研究的性能包括压缩强度、径向拉伸强度和弯曲强度;体外三体磨损;抗断裂性;抛光保持性;以及牙刷磨损后的表面形态。他们使用方差分析/图基 - 克雷默配对分析在95%置信区间进行统计分析。
该纳米复合材料的压缩强度、径向强度和抗断裂性与所测试的其他商用复合材料相当或更高。纳米复合材料体系的三体磨损结果在统计学上优于所有其他测试的复合材料。在延长刷牙时间后,该纳米复合材料的抛光保持性比测试的混合型和微混合型复合材料更好。在延长牙刷磨损后,牙本质色、主体色和牙釉质色的抛光保持性与测试的微填料型相当,而半透明色的抛光保持性比微填料型更好。
所研究的牙科纳米复合材料体系显示出高透明度、高抛光度和类似于微填料型的抛光保持性,同时保持了与几种混合型复合材料相当的物理性能和耐磨性。
所测试的树脂基纳米复合材料的强度和美学性能应使临床医生能够将其用于前牙和后牙修复。