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使用硅烷偶联剂实现树脂粘结水门汀与玻璃渗透氧化铝增强陶瓷之间的粘结。

Bonding between resin luting cement and glass infiltrated alumina-reinforced ceramics with silane coupling agent.

作者信息

Nakamura S, Yoshida K, Kamada K, Atsuta M

机构信息

Division of Fixed Prosthodontics and Oral Rehabilitation, Nagasaki University, Graduate School of Biomedical Sciences, Nagasaki, Japan.

出版信息

J Oral Rehabil. 2004 Aug;31(8):785-9. doi: 10.1111/j.1365-2842.2004.01304.x.

Abstract

The purpose of this study was to evaluate the shear bond strengths of three dual-cured resin luting cements (Linkmax HV, Panavia Fluoro Cement, and RelyX ARC) to glass-infiltrated alumina-reinforced ceramic material and the effect of four silane coupling agents (Clearfil Porcelain Bond, GC Ceramic Primer, Porcelain LinerM, and Tokuso Ceramic Primer) on the bond strength. The two type-shaped of In-Ceram alumina ceramic glass-infiltrated specimens were untreated or treated with one of the four ceramic primers and then cemented together with one of the three dual-cured resin luting cements. Half of the specimens were stored in water at 37 degrees C for 24 h and the other half thermocycled 20,000 times before shear bond strength testing. Surface treatment by all silane coupling agents improved the shear bond strength compared with non-treatment. The specimens treated with Clearfil Porcelain Bond showed significantly greater shear bond strength than any of the other three silane coupling agents regardless of resin luting cements and thermocycling except for the use of Panavia Fluoro Cement at 20,000 thermocycles. When the alumina-reinforced ceramic material was treated with any silane coupling agent except GC Ceramic Primer and cemented with Linkmax HV, no significant differences in bond strength were noted between after water storage and after 20,000 thermocycles. After 20,000 thermocycles, all specimens except for the combined use of Clearfil Porcelain Bond or GC Ceramic Primer and Linkmax HV and GC Ceramic Primer and Panavia Fluoro Cement showed adhesive failures at the ceramic-resin luting cement interface.

摘要

本研究的目的是评估三种双固化树脂粘结水门汀(Linkmax HV、Panavia Fluoro Cement和RelyX ARC)与玻璃渗透氧化铝增强陶瓷材料之间的剪切粘结强度,以及四种硅烷偶联剂(Clearfil Porcelain Bond、GC Ceramic Primer、Porcelain LinerM和Tokuso Ceramic Primer)对粘结强度的影响。将两种形状的In-Ceram氧化铝陶瓷玻璃渗透试件不进行处理或用四种陶瓷底漆之一进行处理,然后用三种双固化树脂粘结水门汀之一粘结在一起。一半试件在37℃水中储存24小时,另一半在进行剪切粘结强度测试前进行20000次热循环。与未处理相比,所有硅烷偶联剂的表面处理均提高了剪切粘结强度。无论使用何种树脂粘结水门汀和是否进行热循环,用Clearfil Porcelain Bond处理的试件均显示出比其他三种硅烷偶联剂显著更高的剪切粘结强度,但在使用Panavia Fluoro Cement进行20000次热循环时除外。当氧化铝增强陶瓷材料用除GC Ceramic Primer之外的任何硅烷偶联剂处理并与Linkmax HV粘结时,储水后和20000次热循环后的粘结强度无显著差异。在20000次热循环后,除了Clearfil Porcelain Bond或GC Ceramic Primer与Linkmax HV以及GC Ceramic Primer与Panavia Fluoro Cement联合使用的试件外,所有试件在陶瓷-树脂粘结水门汀界面均出现粘结破坏。

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