Shindo Daisuke, Hosokawa Masasuke, Liu Zheng, Murakami Yasukazu, Ito Takuya, Iwasaki Yoh, Tachibana Junichi
Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1 Katahira, Sendai-shi 980-8577, Japan.
Microsc Microanal. 2004 Feb;10(1):116-21. doi: 10.1017/S1431927604040218.
The microstructure and magnetic domain structure of a Co-CoO obliquely evaporated tape for magnetic recording are studied by analytical electron microscopy and electron holography, respectively. While the existence of Co and CoO crystallites is confirmed by energy-filtered electron diffraction, columnar structure of the Co crystallites surrounded by the densely packed CoO crystallites is visualized by an elemental mapping method with electron energy loss spectroscopy, and the crystal orientation relation among the Co crystallites is clarified by high-resolution electron microscopy. It is found that the neighboring Co crystallites have close crystal orientations. On the other hand, electron holography reveals the magnetic flux distribution in a thin section of the tape. Although there exists the background resulting from the effect of inner potential with thickness variation, the distribution of lines of magnetic flux is found to correspond well to the recorded pattern.
分别利用分析电子显微镜和电子全息术研究了用于磁记录的Co-CoO倾斜蒸发带的微观结构和磁畴结构。通过能量过滤电子衍射确认了Co和CoO微晶的存在,利用电子能量损失谱的元素映射方法观察到被密集堆积的CoO微晶包围的Co微晶的柱状结构,并用高分辨率电子显微镜阐明了Co微晶之间的晶体取向关系。发现相邻的Co微晶具有相近的晶体取向。另一方面,电子全息术揭示了带材薄片中的磁通量分布。尽管存在由厚度变化引起的内电势效应产生的背景,但发现磁通量线的分布与记录图案非常吻合。