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在50微米内径柱上通过毛细管气相色谱法对超快速精油进行表征。

Ultra-fast essential oil characterization by capillary GC on a 50 microm ID column.

作者信息

Mondello Luigi, Shellie Robert, Casilli Alessandro, Quinto Tranchida Peter, Marriott Philip, Dugo Giovanni

机构信息

Dipartimento Farmaco-chimico, Facoltá di Farmacia, Universitá di Messina, Viale Annunziata, 98168 Messina, Italy

出版信息

J Sep Sci. 2004 Jun;27(9):699-702. doi: 10.1002/jssc.200301602.

Abstract

A 5 m x 50 microm capillary column with 0.05 microm stationary phase film thickness, with a calculated efficiency of almost 20,000 plates per metre (under optimum conditions), was used for very fasthigh resolution GC analysis of lime essential oil. The total analysis time of this volatile essential oil was less than 90 s. Fast GC is shown to be appropriate for essential oil quality assurance analysis, and quantitative results of key components are comparable with those obtained by using conventional GC analysis. The fast GC analysis is approximately 33 times faster than the conventional GC method.

摘要

一根5米长、内径50微米、固定相膜厚0.05微米的毛细管柱,在最佳条件下计算出的柱效约为每米20,000理论塔板数,用于柠檬草精油的超快速高分辨率气相色谱分析。这种挥发性精油的总分析时间不到90秒。结果表明,快速气相色谱适用于精油质量保证分析,关键成分的定量结果与传统气相色谱分析获得的结果相当。快速气相色谱分析比传统气相色谱方法快约33倍。

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