Zhai Yun-bo, Wei Xian-xun, Zeng Guang-ming
Department of Environmental Science and Engineering, Hunan University, Changsha 410082, China.
J Environ Sci (China). 2004;16(4):683-6.
According to the Doehlert's matrix method, the adsorbent derived from sewage sludge was prepared through chemical activation under controlling the pyrolysis temperature and hold time. The characteristic parameters including the total yield, adsorption of methylene blue, adsorption of iodine, BET surface area, micro-pore volume are 35%--49%, 16.5--38 mg/g, 285--362 mg/g, 185--359 m2/g, and 0.112--0.224 m3/g, respectively. According to the experimental data, the multi-linear regression method was adopted to fit the relations between the characteristic parameters and influential factors. At final, through optimization method, the optimal adsorbent is obtained when using 62 min as hold time and 1105K as pyrolysis temperature. Under the conditions, the adsorbent was produced and compared the characteristic parameters with model forecast value, the coherence is satisfied.
根据多尔勒特矩阵法,在控制热解温度和保温时间的条件下,通过化学活化制备了源自污水污泥的吸附剂。包括总产率、亚甲基蓝吸附量、碘吸附量、BET比表面积、微孔体积在内的特征参数分别为35% - 49%、16.5 - 38mg/g、285 - 362mg/g、185 - 359m²/g和0.112 - 0.224m³/g。根据实验数据,采用多元线性回归方法拟合特征参数与影响因素之间的关系。最后,通过优化方法,当保温时间为62分钟、热解温度为1105K时获得了最佳吸附剂。在此条件下制备了吸附剂,并将特征参数与模型预测值进行比较,一致性令人满意。