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正交试验在电感耦合等离子体发射光谱法测定野菜中微量元素的应用

[Application of orthogonal test in determination of trace elements in wild vegetables by ICP-AES].

作者信息

Wang Ying, Xin Shi-gang

机构信息

Chemistry and Life Science College, Shenyang Normal College, Shenyang 110034, China.

出版信息

Guang Pu Xue Yu Guang Pu Fen Xi. 2004 Oct;24(10):1253-6.

Abstract

In this paper, orthogonal test was applied to determination of trace elements in wild vegetables just as Mn, Se, Cu, Fe, Mg and Zn by ICP-AES. It could provide many informations for us by less experimental times, and could choice the best experimental conditions by square-error analysis. It would be helpful for improving experimental accuracy. The method was simple, rapid, and possessed of highly sensitivity, good accuracy and determination of many elements at the same time, in addition little environment pollution. The recoveries of the method were in the range of 97.2%-103.3%, and relative standard deviations were less than 2.15%. The experimental results proved wild vegetables were valuable and nutritious food, they had rich trace elements.

摘要

本文采用正交试验,通过电感耦合等离子体发射光谱法(ICP - AES)测定野生蔬菜中的微量元素,如锰、硒、铜、铁、镁和锌。该方法能以较少的实验次数为我们提供大量信息,并通过方差分析选择最佳实验条件,有助于提高实验准确性。该方法简便、快速,具有高灵敏度、良好的准确度且能同时测定多种元素,此外环境污染小。该方法的回收率在97.2% - 103.3%范围内,相对标准偏差小于2.15%。实验结果证明野生蔬菜是有价值且营养丰富的食物,它们含有丰富的微量元素。

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