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[氢化物发生-电感耦合等离子体发射光谱法测定麦冬中的微量元素]

[Determination of trace elements in radix ophiopogonis by HG-ICP-AES].

作者信息

Lou Qi-Zheng, Xu Run-Sheng

机构信息

Department of Biology and Chemistry, Jinhua Education College, Jinhua 321000, China.

出版信息

Guang Pu Xue Yu Guang Pu Fen Xi. 2007 Jun;27(6):1218-21.

Abstract

In this paper, a method of microwave digestion technique for the contents determination of trace elements Ni, Zn, Mn, Cu, Mg, Fe, Ca and Pb in radix ophiopogonis by hydride generation inductively coupled plasma atomic emition spectrometry (HG-ICP-AES) was reported. Its recovery ratio obtained by standard addition method ranged between 97.8% and 102.5%, and its RSD was lower than 4.0%. The results of the determination show that radix ophiopogonis is rich in the inorganic elements such as Fe, and the content of Zn in radix ophiopogonis of Zhejiang is much higher in radix ophiopogonis of Sichun. The result will provide scientific data for the study on the elements in radix ophiopogonis and on their relativity of medicine efficacy.

摘要

本文报道了一种采用氢化物发生电感耦合等离子体原子发射光谱法(HG-ICP-AES)测定麦冬中微量元素镍、锌、锰、铜、镁、铁、钙和铅含量的微波消解技术方法。采用标准加入法测得其回收率在97.8%至102.5%之间,相对标准偏差低于4.0%。测定结果表明,麦冬富含铁等无机元素,浙江麦冬中锌的含量远高于四川麦冬。该结果将为麦冬中元素及其与药效相关性的研究提供科学数据。

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