确定十种苯基哌嗪衍生物的¹H和¹³C核磁共振数据。
Complete assignments of 1H and 13C NMR data for ten phenylpiperazine derivatives.
作者信息
Xiao Zhihui, Yuan Mu, Zhang Si, Wu Jun, Qi Shuhua, Li Qingxin
机构信息
Guangdong Key Laboratory of Marine Materia Medica, South China Sea Institute of Oceanology, Chinese Academy of Sciences, Guangzhou 510301, China.
出版信息
Magn Reson Chem. 2005 Oct;43(10):869-72. doi: 10.1002/mrc.1641.
DOI:10.1002/mrc.1641
PMID:16041776
Abstract
Ten phenylpiperazine derivatives were designed and synthesized. The first complete assignments of (1)H and (13)C NMR chemical shifts for these phenylpiperazine derivatives were achieved by means of 1D and 2D NMR techniques, including (1)H-(1)H COSY, HSQC and HMBC spectra.
摘要
设计并合成了十种苯基哌嗪衍生物。借助一维和二维核磁共振技术，包括氢-氢化学位移相关谱（1H-1H COSY）、异核单量子相干谱（HSQC）和异核多键相关谱（HMBC），首次完成了这些苯基哌嗪衍生物的氢核磁共振（1H NMR）和碳核磁共振（13C NMR）化学位移的全归属。
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