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通过中子活化分析对药用植物嘉赐树中的微量元素进行表征。

Characterization of trace elements in Casearia medicinal plant by neutron activation analysis.

作者信息

Yamashita C I, Saiki M, Vasconcellos M B A, Sertié J A A

机构信息

Neutron Activation Analysis Laboratory, IPEN-CNEN/SP, Av. Prof. Lineu Prestes 2242, CEP 05508-000, São Paulo, SP, Brazil.

出版信息

Appl Radiat Isot. 2005 Nov-Dec;63(5-6):841-6. doi: 10.1016/j.apradiso.2005.05.045. Epub 2005 Aug 15.

Abstract

Leaves of Casearia sylvestris, Casearia decandra and Casearia obliqua plant species, collected at the Atlantic Forest in Brazil, were analyzed by using instrumental neutron activation analysis (INAA). Short and long irradiations using thermal neutron flux of the IEA-R1 nuclear reactor were carried out for these analyses. Concentrations of Ca, K and Mg were found in these samples at the percentage levels, Br, Cl, Fe, Mn, Na, Rb and Zn at the microg g(-1) levels and Co, Cr, Cs, La, and Sc at the microg kg(-1) levels. Comparisons were made among the element concentrations obtained in these three Casearia species and significant differences were found for the elements Cl, Co, Cs, Cr, La, Mn, Na and Sc. The precision and the accuracy of the results were evaluated by analyzing the certified reference materials NIST-1515 Apple Leaves and NIST-1573a Tomato Leaves.

摘要

对采集自巴西大西洋森林的野生嘉赐树、十蕊嘉赐树和斜叶嘉赐树的叶子,采用仪器中子活化分析(INAA)进行了分析。为这些分析使用国际原子能机构R1核反应堆的热中子通量进行了短时间和长时间辐照。在这些样品中发现,钙、钾和镁的浓度为百分比水平,溴、氯、铁、锰、钠、铷和锌的浓度为微克/克(-1)水平,钴、铬、铯、镧和钪的浓度为微克/千克(-1)水平。对这三种嘉赐树物种获得的元素浓度进行了比较,发现氯、钴、铯、铬、镧、锰、钠和钪等元素存在显著差异。通过分析标准参考物质NIST-1515苹果叶和NIST-1573a番茄叶对结果的精密度和准确性进行了评估。

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