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发光二极管固化灯的光散射对树脂复合材料聚合的影响。

Effect of light dispersion of LED curing lights on resin composite polymerization.

作者信息

Vandewalle Kraig S, Roberts Howard W, Andrus Jeffrey L, Dunn William J

机构信息

Dental Materials and Testing, USAF Dental Investigation Service, Great Lakes, IL 60088, USA.

出版信息

J Esthet Restor Dent. 2005;17(4):244-54; discussion 254-5. doi: 10.1111/j.1708-8240.2005.tb00122.x.

Abstract

PURPOSE

This study evaluated the effect of light dispersion of halogen and LED curing lights on resin composite polymerization.

MATERIALS AND METHODS

One halogen (Optilux 501, SDS/Kerr, Orange, CA, USA) and five light-emitting diode (LED) curing lights (SmartLite iQ, Dentsply Caulk, Milford, DE, USA; LEDemetron 1, SDS/Kerr; FLASHlite 1001, Discus Dental, Culver City, CA, USA; UltraLume LED 5, Ultradent Products, South Jordan, UT, USA; Allegro, Den-Mat, Santa Maria, CA, USA) were used in this study. Specimens (8 mm diameter by 2 mm thick) were made in polytetrafluoroethylene molds using hybrid (Z100, 3M ESPE, St. Paul, MN, USA) and microfill (A110, 3M ESPE) composite resins. The top surface was polymerized for 5 seconds with the curing light guide tip positioned at a distance of 1 and 5 mm. Degree of conversion (DC) of the composite specimens was analyzed on the bottom surface using micro-Fourier Transform Infrared (FTIR) spectroscopy (Perkin-Elmer FTIR Spectrometer, Wellesley, PA, USA) 10 minutes after light activation. DC at the bottom of the 2 mm specimen was expressed as a percentage of the mean maximum DC. Five specimens were created per curing light and composite type (n=5). Percent mean DC ratios and SDs were calculated for each light under each testing condition. Data were analyzed by analysis of variance (ANOVA)/Tukey's test (alpha = .05). A beam analyzer (LBA-700, Spiricon, Logan, UT, USA) was used to record the emitted light from the curing lights at 0 and 5 mm distances (n=5). A Top Hat factor was used to compare the quality of the emitted beam profile (LBA/PC, Spiricon). The divergence angle from vertical was also determined in the x- and y-axes (LBA/PC). Mean values and SDs were calculated for each light under each testing condition (0 and 5 mm, x- and y-axes) and analyzed by a two-way ANOVA/Tukey's test (alpha = .05).

RESULTS

For DC ratios, significant differences were found based on curing light and curing distance (p < .05). At 1 mm, Optilux 501 and FLASHlite 1001 produced significantly higher DC ratios with the hybrid resin composite. No differences were found among lights with the microfill at 1 mm. At 5 mm, SmartLite iQ, FLASHlite 1001, LEDemetron 1, and UltraLume LED 5 produced significantly higher DC ratios with the hybrid resin composite, whereas LEDemetron 1 and SmartLite iQ produced significantly higher DC ratios with the microfill resin composite. The UltraLume LED 5, Allegro, and Optilux 501 had significant reductions in mean DC ratios at curing distances of 1 and 5 mm with both resin composite types. For dispersion of light, significant differences were found in Top Hat factor and divergence angle (p < .001). SmartLite iQ had overall the highest Top Hat factor and lowest divergence angle of tested lights. A linear regression analysis relating pooled DC with pooled Top Hat factors and divergence angles found a very good correlation (r2 = .86) between dispersion of light over distance and the ability to polymerize resin composite.

CLINICAL SIGNIFICANCE

The latest generation of LED curing lights provides DC ratios similar to or better than the halogen curing light at a curing distance of 5 mm. Dispersion of light plays a significant role in the DC of resin composite. To maximize curing effectiveness, light guides should be maintained in close proximity to the surface of the light-activated restorative material.

摘要

目的

本研究评估了卤素固化灯和发光二极管(LED)固化灯的光散射对树脂复合材料聚合的影响。

材料与方法

本研究使用了一台卤素固化灯(Optilux 501,SDS/Kerr,美国加利福尼亚州奥兰治)和五台发光二极管固化灯(SmartLite iQ,登士柏卡沃,美国特拉华州米尔福德;LEDemetron 1,SDS/Kerr;FLASHlite 1001,迪氏牙科,美国加利福尼亚州卡尔弗城;UltraLume LED 5,Ultradent Products,美国犹他州南乔丹;Allegro,丹马特,美国加利福尼亚州圣玛丽亚)。使用混合树脂(Z100,3M ESPE,美国明尼苏达州圣保罗)和微填料树脂(A110,3M ESPE)在聚四氟乙烯模具中制作样本(直径8mm,厚2mm)。将固化光导尖端置于距离样本顶面1mm和5mm处,对顶面进行5秒的聚合照射。光激活10分钟后,使用微型傅里叶变换红外光谱仪(Perkin-Elmer FTIR光谱仪,美国宾夕法尼亚州韦尔斯利)在样本底面分析复合材料样本的转化率(DC)。2mm样本底部的DC表示为平均最大DC的百分比。每种固化灯和复合材料类型制作五个样本(n = 5)。计算每种测试条件下每种固化灯的平均DC百分比和标准差。数据采用方差分析(ANOVA)/Tukey检验进行分析(α = 0.05)。使用光束分析仪(LBA - 700,Spiricon,美国犹他州洛根)记录固化灯在0mm和5mm距离处发出的光(n = 5)。使用顶帽因子比较发出光束轮廓的质量(LBA / PC,Spiricon)。还在x轴和y轴上确定与垂直方向的发散角(LBA / PC)。计算每种测试条件(0mm和mm,x轴和y轴)下每种固化灯的平均值和标准差,并通过双向ANOVA / Tukey检验进行分析(α = 0.05)。

结果

对于DC比率,基于固化灯和固化距离发现了显著差异(p < 0.05)。在1mm处,Optilux 501和FLASHlite 1001与混合树脂复合材料产生的DC比率显著更高。在1mm处,微填料树脂复合材料的不同固化灯之间未发现差异。在5mm处,SmartLite iQ、FLASHlite 1001、LEDemetron 1和UltraLume LED 5与混合树脂复合材料产生的DC比率显著更高,而LEDemetron 1和SmartLite iQ与微填料树脂复合材料产生的DC比率显著更高。对于两种树脂复合材料类型,UltraLume LED 5、Allegro和Optilux 501在1mm和5mm的固化距离下平均DC比率显著降低。对于光散射,在顶帽因子和发散角方面发现了显著差异(p < 0.001)。SmartLite iQ在测试的固化灯中总体上具有最高的顶帽因子和最低的发散角。对合并的DC与合并的顶帽因子和发散角进行线性回归分析发现,光在距离上的散射与树脂复合材料的聚合能力之间存在非常好的相关性(r2 = 0.86)。

临床意义

最新一代的LED固化灯在5mm的固化距离下提供的DC比率与卤素固化灯相似或更好。光散射在树脂复合材料的DC中起重要作用。为了使固化效果最大化,光导应保持靠近光激活修复材料的表面。

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