Biswas Mousumi, Mazumdar Dibyendu
Department of Conservative Dentistry and Endodontics, Dr. R. Ahmed Dental College and Hospital, Kolkata, West Bengal, India.
J Conserv Dent Endod. 2023 Sep-Oct;26(5):530-538. doi: 10.4103/JCDE.JCDE_48_23. Epub 2023 Sep 16.
The purpose of our study was to determine the amount of eluted triethyleneglycol dimethacrylate (TEGDMA) and to compare the eluted TEGDMA in different composite resins after light curing with conventional halogen light curing unit and light emitting diode (LED).
The present study was conducted on the two types of composite resins, which were divided equally into four groups - Group I: Denoted as Hybrid-LED, Group II: Denoted as Microhybrid-LED, Group III: Denoted as Hybrid-Halogen Group IV: Denoted as Microhybrid-Halogen. Polymerized specimens of hybrid and microhybrid composite resins were stored in air tight centrifuge tubes at 37°C for 24 h, then extract the monomers in high-performance liquid chromatography (HPLC) grade acetonitrile and water and incubated at 37°C for 24 h. All extracts were analyzed by HPLC. Eluted TEGDMA was detected by ultraviolet detector. The results obtained for TEGDMA were computed and analyzed using the one-way ANOVA and independent samples -test at significance level 0.05.
Elution of TEGDMA from all the samples of Group III (Hybrid-Halogen) was greatest and from Group II (Microhybrid-LED) was lowest. The sequence of TEGDMA elution was Group III > Group I > Group IV > Group II. From our results, we can conclude that the LED light curing unit may be more efficient than standard halogen light curing unit. The extractable quantities of composite resin components should be minimized. Furthermore, all ingredients of a dental composite should be declared by the manufacturers, in order to identify those substances in a product which may cause adverse side effects in patients and dental personnel.
本研究的目的是确定洗脱的三乙二醇二甲基丙烯酸酯(TEGDMA)的量,并比较使用传统卤素光固化装置和发光二极管(LED)光固化后不同复合树脂中洗脱的TEGDMA。
本研究针对两种类型的复合树脂进行,将其平均分为四组——第一组:标记为混合-LED组;第二组:标记为微混合-LED组;第三组:标记为混合-卤素组;第四组:标记为微混合-卤素组。将混合和微混合复合树脂的聚合标本在37°C下密封于离心管中保存24小时,然后在高效液相色谱(HPLC)级乙腈和水中提取单体,并在37°C下孵育24小时。所有提取物均通过HPLC进行分析。通过紫外检测器检测洗脱的TEGDMA。使用单因素方差分析和独立样本检验对TEGDMA的结果进行计算和分析,显著性水平为0.05。
第三组(混合-卤素组)所有样本中TEGDMA的洗脱量最大,第二组(微混合-LED组)最低。TEGDMA洗脱顺序为第三组>第一组>第四组>第二组。从我们的结果可以得出结论,LED光固化装置可能比标准卤素光固化装置更有效。复合树脂成分的可提取量应降至最低。此外,牙科复合材料的所有成分应由制造商声明,以便识别产品中可能对患者和牙科人员造成不良副作用的那些物质。